trans-3-phenyl-2-propenyl 2-acetamido-(R)-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:trans-3-phenyl-2-propenyl 2-acetamido-(R)-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside
CAS No.:508194-11-4
Molecular Formula:C₂₄H₂₇NO₆
Molecular Weight:425.481
Hs Code.:

Synonyms:trans-3-phenyl-2-propenyl 2-acetamido-(R)-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

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Chemical Property of trans-3-phenyl-2-propenyl 2-acetamido-(R)-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

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Technology Process of trans-3-phenyl-2-propenyl 2-acetamido-(R)-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

There total 5 articles about trans-3-phenyl-2-propenyl 2-acetamido-(R)-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4407-36-7
(2E)-3-phenyl-2-propen-1-ol

: 508194-11-4
trans-3-phenyl-2-propenyl 2-acetamido-(R)-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / molecular sieves 4 Angstroem; Hg(CN)2 / nitromethane; toluene / 20 °C

2: NaOMe / methanol / 0.5 h / 20 °C

3: 9.2 g / ZnCl₂ / 48 h

With 4 A molecular sieve; sodium methylate; mercury(II) cyanide; zinc(II) chloride; In methanol; nitromethane; toluene;
DOI:10.1016/S0957-4166(02)00649-3

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 194035-36-4
N-[(2R,3R,4R,5S,6R)-4,5-Dihydroxy-6-hydroxymethyl-2-((E)-3-phenyl-allyloxy)-tetrahydro-pyran-3-yl]-acetamide

: 508194-11-4
trans-3-phenyl-2-propenyl 2-acetamido-(R)-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

Guidance literature:: With camphor-10-sulfonic acid; In acetonitrile; at 20 ℃;
DOI:10.1002/ejoc.201101539

Reference yield:

: 508194-07-8
trans-3-phenyl-2-propenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

: 508194-11-4
trans-3-phenyl-2-propenyl 2-acetamido-(R)-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: NaOMe / methanol / 0.5 h / 20 °C

2: 9.2 g / ZnCl₂ / 48 h

With sodium methylate; zinc(II) chloride; In methanol;
DOI:10.1016/S0957-4166(02)00649-3