(S)-S-3-(benzyloxycarbonylamino)-4-oxo-4-(5-oxopentylamino)butylethanethioate

Base Information

Chemical Name:(S)-S-3-(benzyloxycarbonylamino)-4-oxo-4-(5-oxopentylamino)butylethanethioate
CAS No.:1400677-20-4
Molecular Formula:C₁₉H₂₆N₂O₅S
Molecular Weight:394.492
Hs Code.:

Synonyms:(S)-S-3-(benzyloxycarbonylamino)-4-oxo-4-(5-oxopentylamino)butylethanethioate

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Chemical Property of (S)-S-3-(benzyloxycarbonylamino)-4-oxo-4-(5-oxopentylamino)butylethanethioate

Chemical Property:

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Technology Process of (S)-S-3-(benzyloxycarbonylamino)-4-oxo-4-(5-oxopentylamino)butylethanethioate

There total 3 articles about (S)-S-3-(benzyloxycarbonylamino)-4-oxo-4-(5-oxopentylamino)butylethanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1400677-19-1
(S)-S-3-(benzyloxycarbonylamino)-4-(5-hydroxypentylamino)-4-oxobutylethanethioate

: 1400677-20-4
(S)-S-3-(benzyloxycarbonylamino)-4-oxo-4-(5-oxopentylamino)butylethanethioate

Guidance literature:: (S)-S-3-(benzyloxycarbonylamino)-4-(5-hydroxypentylamino)-4-oxobutylethanethioate; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.75h;

With triethylamine; In dichloromethane; at -35 - -30 ℃; for 1h;

Reference yield:

: 167305-82-0
(S)-4-(acetylthio)-2-(benzyloxycarbonylamino)butanoic acid

: 1400677-20-4
(S)-S-3-(benzyloxycarbonylamino)-4-oxo-4-(5-oxopentylamino)butylethanethioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 16 h / 20 °C

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

2.2: 1 h / -35 - -30 °C

With oxalyl dichloride; benzotriazol-1-ol; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;

Reference yield:

: 2508-29-4
5-hydroxypentylamine

: 1400677-20-4
(S)-S-3-(benzyloxycarbonylamino)-4-oxo-4-(5-oxopentylamino)butylethanethioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 16 h / 20 °C

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

2.2: 1 h / -35 - -30 °C

With oxalyl dichloride; benzotriazol-1-ol; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;