5-bromomethyl-3-(p-toluyl)-Δ2-isoxazoline

Base Information

Chemical Name:5-bromomethyl-3-(p-toluyl)-Δ2-isoxazoline
CAS No.:1191925-09-3
Molecular Formula:C₁₁H₁₂BrNO
Molecular Weight:254.126
Hs Code.:

Synonyms:5-bromomethyl-3-(p-toluyl)-Δ2-isoxazoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-bromomethyl-3-(p-toluyl)-Δ2-isoxazoline

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Technology Process of 5-bromomethyl-3-(p-toluyl)-Δ2-isoxazoline

There total 4 articles about 5-bromomethyl-3-(p-toluyl)-Δ2-isoxazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 904672-45-3
1-(p-tolyl)-3-buten-1-one oxime

: 1191925-09-3
5-bromomethyl-3-(p-toluyl)-Δ2-isoxazoline

Guidance literature:: With tert.-butylnitrite; carbon tetrabromide; In tetrahydrofuran; at 20 ℃; for 0.333333h; Schlenk technique; Inert atmosphere;
DOI:10.1039/c6ob01374k

Reference yield:

: 104-87-0
4-methyl-benzaldehyde

: 1191925-09-3
5-bromomethyl-3-(p-toluyl)-Δ2-isoxazoline

Guidance literature:: Multi-step reaction with 4 steps

1: diethyl ether / 0 - 20 °C

2: Jones reagent / diethyl ether / 1 h / 0 - 20 °C

3: hydroxylamine hydrochloride; sodium acetate / water; ethanol / 20 °C

4: palladium diacetate; copper dichloride / dimethyl sulfoxide / 8 h / 20 °C / Inert atmosphere

With Jones reagent; hydroxylamine hydrochloride; sodium acetate; palladium diacetate; copper dichloride; In diethyl ether; ethanol; water; dimethyl sulfoxide;
DOI:10.1002/ejoc.201403538

Reference yield:

: 24165-63-7
1-p-tolyl-3-buten-1-ol

: 1191925-09-3
5-bromomethyl-3-(p-toluyl)-Δ2-isoxazoline

Guidance literature:: Multi-step reaction with 3 steps

1: Jones reagent / diethyl ether / 1 h / 0 - 20 °C

2: hydroxylamine hydrochloride; sodium acetate / water; ethanol / 20 °C

3: palladium diacetate; copper dichloride / dimethyl sulfoxide / 8 h / 20 °C / Inert atmosphere

With Jones reagent; hydroxylamine hydrochloride; sodium acetate; palladium diacetate; copper dichloride; In diethyl ether; ethanol; water; dimethyl sulfoxide;
DOI:10.1002/ejoc.201403538