1'-C-(2-O-acetyl-3,4,6-tri-O-benzoyl-2S-cyano-β-D-glucopyranosyl)acetophenone

Base Information

Chemical Name:1'-C-(2-O-acetyl-3,4,6-tri-O-benzoyl-2S-cyano-β-D-glucopyranosyl)acetophenone
CAS No.:127863-20-1
Molecular Formula:C₃₈H₃₁NO₁₀
Molecular Weight:661.665
Hs Code.:

Synonyms:1'-C-(2-O-acetyl-3,4,6-tri-O-benzoyl-2S-cyano-β-D-glucopyranosyl)acetophenone

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Chemical Property of 1'-C-(2-O-acetyl-3,4,6-tri-O-benzoyl-2S-cyano-β-D-glucopyranosyl)acetophenone

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Technology Process of 1'-C-(2-O-acetyl-3,4,6-tri-O-benzoyl-2S-cyano-β-D-glucopyranosyl)acetophenone

There total 3 articles about 1'-C-(2-O-acetyl-3,4,6-tri-O-benzoyl-2S-cyano-β-D-glucopyranosyl)acetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 13735-81-4
1-styrenyloxytrimethylsilane

: 128995-29-9
2-O-acetyl-3,4,6-tri-O-benzoyl-2S-cyano-α-D-glucopyranosyl bromide

: 127863-20-1
1'-C-(2-O-acetyl-3,4,6-tri-O-benzoyl-2S-cyano-β-D-glucopyranosyl)acetophenone

Guidance literature:: With silver trifluoromethanesulfonate; In dichloromethane; for 7h;
DOI:10.1002/ejoc.200300152

Reference yield:

: 82469-69-0
3,4,6-tri-O-benzoyl-α-D-arabino-hexopyranosyl-2-ulose bromide

: 127863-20-1
1'-C-(2-O-acetyl-3,4,6-tri-O-benzoyl-2S-cyano-β-D-glucopyranosyl)acetophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / CH₂Cl₂ / 4 h / 20 °C

2: 93 percent / BF₃-diethyl ether / 3 h / 20 °C

3: 81 percent / silver triflate / CH₂Cl₂ / 7 h

With boron trifluoride diethyl etherate; silver trifluoromethanesulfonate; In dichloromethane;
DOI:10.1002/ejoc.200300152

Reference yield:

: 127844-88-6
3,4,6-tri-O-benzoyl-2S-cyano-α-D-glucopyranosyl bromide

: 127863-20-1
1'-C-(2-O-acetyl-3,4,6-tri-O-benzoyl-2S-cyano-β-D-glucopyranosyl)acetophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / BF₃-diethyl ether / 3 h / 20 °C

2: 81 percent / silver triflate / CH₂Cl₂ / 7 h

With boron trifluoride diethyl etherate; silver trifluoromethanesulfonate; In dichloromethane;
DOI:10.1002/ejoc.200300152