cyclohexa-1,3-dien-1-ylmethyl acetate

Base Information

Chemical Name:cyclohexa-1,3-dien-1-ylmethyl acetate
CAS No.:32833-06-0
Molecular Formula:C₉H₁₂O₂
Molecular Weight:152.193
Hs Code.:

Synonyms:cyclohexa-1,3-dien-1-ylmethyl acetate

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Chemical Property of cyclohexa-1,3-dien-1-ylmethyl acetate

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Technology Process of cyclohexa-1,3-dien-1-ylmethyl acetate

There total 2 articles about cyclohexa-1,3-dien-1-ylmethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 21203-48-5
1,3-cyclohexadiene-1-methanol

: 108-24-7
acetic anhydride

: 32833-06-0
cyclohexa-1,3-dien-1-ylmethyl acetate

Guidance literature:: With dmap; In dichloromethane; at 0 - 20 ℃; for 18h; Inert atmosphere;
DOI:10.3762/bjoc.13.41

Reference yield:

: 1121-54-6
1,3-Cyclohexadiene-1-carbaldehyde

: 32833-06-0
cyclohexa-1,3-dien-1-ylmethyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / methanol; H₂O

2: NaH / 1,2-dimethoxy-ethane

With sodium tetrahydroborate; sodium hydride; In methanol; 1,2-dimethoxyethane; water;

Reference yield: 16.0%

: 110-44-1,91751-55-2
sorbic Acid

: 32833-06-0
cyclohexa-1,3-dien-1-ylmethyl acetate

: 3-methylene-6-((1E,3E)-penta-1,3-dien-1-yl)cyclohex-1-ene

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; water; triphenylphosphine; In chloroform-d1; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.3762/bjoc.13.41