5-phenyl-2-thioxo-2,3,6,7,8,9-hexahydro-1H-pyrimido[4,5-b]quinolin-4-one

Base Information

• Chemical Name: 5-phenyl-2-thioxo-2,3,6,7,8,9-hexahydro-1H-pyrimido[4,5-b]quinolin-4-one
• CAS No.: 1024582-41-9
• Molecular Formula: C₁₇H₁₅N₃OS
• Molecular Weight: 309.392

Synonyms:5-phenyl-2-thioxo-2,3,6,7,8,9-hexahydro-1H-pyrimido[4,5-b]quinolin-4-one

Chemical Property of 5-phenyl-2-thioxo-2,3,6,7,8,9-hexahydro-1H-pyrimido[4,5-b]quinolin-4-one

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Technology Process of 5-phenyl-2-thioxo-2,3,6,7,8,9-hexahydro-1H-pyrimido[4,5-b]quinolin-4-one

There total 3 articles about 5-phenyl-2-thioxo-2,3,6,7,8,9-hexahydro-1H-pyrimido[4,5-b]quinolin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

6-Amino-2-thiouracil (1004-40-6) + 2-Benzylidenecyclohexanone (5682-83-7) → 5-phenyl-2-thioxo-2,3,6,7,8,9-hexahydro-1H-pyrimido[4,5-b]quinolin-4-one (1024582-41-9)

Guidance literature:

In N,N-dimethyl-formamide; Heating; prolonged reaction time;

DOI:10.1016/j.bmc.2007.12.012

Reference yield: 63.0%

6-Amino-2-thiouracil (1004-40-6) + 2-Benzylidenecyclohexanone (5682-83-7) → 5-phenyl-2-thioxo-2,3,6,7,8,9-hexahydro-1H-pyrimido[4,5-b]quinolin-4-one (1024582-41-9) + C17H17N3OS (1024582-36-2)

Guidance literature:

In N,N-dimethyl-formamide; Heating;

DOI:10.1016/j.bmc.2007.12.012

Reference yield:

6-Amino-2-thiouracil (1004-40-6) + cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + benzaldehyde (100-52-7) → 5-phenyl-2-thioxo-2,3,6,7,8,9-hexahydro-1H-pyrimido[4,5-b]quinolin-4-one (1024582-41-9) + C17H17N3OS (1024582-36-2)

Guidance literature:

In N,N-dimethyl-formamide; Heating;

DOI:10.1016/j.bmc.2007.12.012

upstream raw materials:

6-Amino-2-thiouracil

cyclohexanone

benzaldehyde

2-Benzylidenecyclohexanone

Downstream raw materials:

3-acetyl-1-(4-chlorophenyl)-6-phenyl-7,8,9,10-tetrahydrotriazolo[4',3':1,2]-pyrimido[4,5-b]quinolin-5-one

3-acetyl-1-(4-nitroxyphenyl)-6-phenyl-7,8,9,10-tetrahydrotriazolo[4',3':1,2]-pyrimido[4,5-b]quinolin-5-one

C₁₇H₁₇N₅O

C₃₀H₂₃N₅O

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