5-(N-Boc-L-phenylalaninlyamido)-5-deoxy-1,2-O-isopropylidene-α-D-xylofuranose

Base Information

• Chemical Name: 5-(N-Boc-L-phenylalaninlyamido)-5-deoxy-1,2-O-isopropylidene-α-D-xylofuranose
• CAS No.: 1361249-75-3
• Molecular Formula: C₂₂H₃₂N₂O₇
• Molecular Weight: 436.505

Synonyms:5-(N-Boc-L-phenylalaninlyamido)-5-deoxy-1,2-O-isopropylidene-α-D-xylofuranose

Chemical Property of 5-(N-Boc-L-phenylalaninlyamido)-5-deoxy-1,2-O-isopropylidene-α-D-xylofuranose

Chemical Property:

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Technology Process of 5-(N-Boc-L-phenylalaninlyamido)-5-deoxy-1,2-O-isopropylidene-α-D-xylofuranose

There total 1 articles about 5-(N-Boc-L-phenylalaninlyamido)-5-deoxy-1,2-O-isopropylidene-α-D-xylofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

N-tert-butoxycarbonyl-L-phenylalanine (13734-34-4) + 5-amino-5-deoxy-1,2-O-isopropylidene-a-D-xylofuranose (4613-58-5,25531-86-6,25572-88-7) → 5-(N-Boc-L-phenylalaninlyamido)-5-deoxy-1,2-O-isopropylidene-α-D-xylofuranose (1361249-75-3)

Guidance literature:

N-tert-butoxycarbonyl-L-phenylalanine; With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; at -15 ℃; Inert atmosphere;

5-amino-5-deoxy-1,2-O-isopropylidene-a-D-xylofuranose; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1002/adsc.201100766

Reference yield: 48.0%

5-(N-Boc-L-phenylalaninlyamido)-5-deoxy-1,2-O-isopropylidene-α-D-xylofuranose (1361249-75-3) + benzoyl chloride (98-88-4) → C29H36N2O8 (1361249-91-3)

Guidance literature:

With pyridine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1002/adsc.201100766

Reference yield:

5-(N-Boc-L-phenylalaninlyamido)-5-deoxy-1,2-O-isopropylidene-α-D-xylofuranose (1361249-75-3) → C17H24N2O5

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 4h;

DOI:10.1016/j.jorganchem.2014.10.002

upstream raw materials:

N-tert-butoxycarbonyl-L-phenylalanine

5-amino-5-deoxy-1,2-O-isopropylidene-a-D-xylofuranose

Downstream raw materials:

C₂₉H₃₆N₂O₈

C₂₉H₃₆N₂O₇S

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