trifluoromethanesulfonic acid 4-{1-[4-(3,3-dimethyl-2-oxo-butoxy)-3-methyl-phenyl]-1-ethylpropyl}-2-methyl-phenyl ester

Base Information

• Chemical Name: trifluoromethanesulfonic acid 4-{1-[4-(3,3-dimethyl-2-oxo-butoxy)-3-methyl-phenyl]-1-ethylpropyl}-2-methyl-phenyl ester
• CAS No.: 700832-39-9
• Molecular Formula: C₂₆H₃₃F₃O₅S
• Molecular Weight: 514.606

Synonyms:trifluoromethanesulfonic acid 4-{1-[4-(3,3-dimethyl-2-oxo-butoxy)-3-methyl-phenyl]-1-ethylpropyl}-2-methyl-phenyl ester

Chemical Property of trifluoromethanesulfonic acid 4-{1-[4-(3,3-dimethyl-2-oxo-butoxy)-3-methyl-phenyl]-1-ethylpropyl}-2-methyl-phenyl ester

Chemical Property:

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Technology Process of trifluoromethanesulfonic acid 4-{1-[4-(3,3-dimethyl-2-oxo-butoxy)-3-methyl-phenyl]-1-ethylpropyl}-2-methyl-phenyl ester

There total 4 articles about trifluoromethanesulfonic acid 4-{1-[4-(3,3-dimethyl-2-oxo-butoxy)-3-methyl-phenyl]-1-ethylpropyl}-2-methyl-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

trifluoromethylsulfonic anhydride (358-23-6) + 1-(4-(3-(4-hydroxy-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)-3,3-dimethylbutan-2-one (233268-82-1) → trifluoromethanesulfonic acid 4-{1-[4-(3,3-dimethyl-2-oxo-butoxy)-3-methyl-phenyl]-1-ethylpropyl}-2-methyl-phenyl ester (700832-39-9)

Guidance literature:

With pyridine; at 0 - 20 ℃;

Reference yield: 98.0%

1-(4-(3-(4-hydroxy-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)-3,3-dimethylbutan-2-one (233268-82-1) → trifluoromethanesulfonic acid 4-{1-[4-(3,3-dimethyl-2-oxo-butoxy)-3-methyl-phenyl]-1-ethylpropyl}-2-methyl-phenyl ester (700832-39-9)

Guidance literature:

With pyridine; trifluoromethylsulfonic anhydride; at 0 - 20 ℃; for 14h;

Reference yield: 83.0%

trifluoromethanesulfonic acid 4-[1-ethyl-1-(4-hydroxy-3-methylphenyl)-propyl]-2-methylphenyl ester (865235-89-8) + 1-chloro-3,3-dimethyl-butan-2-one (13547-70-1) → trifluoromethanesulfonic acid 4-{1-[4-(3,3-dimethyl-2-oxo-butoxy)-3-methyl-phenyl]-1-ethylpropyl}-2-methyl-phenyl ester (700832-39-9)

Guidance literature:

With potassium carbonate; In acetone; for 17h; Heating / reflux;

upstream raw materials:

trifluoromethanesulfonic acid 4-[1-ethyl-1-(4-hydroxy-3-methylphenyl)-propyl]-2-methylphenyl ester

1-chloro-3,3-dimethyl-butan-2-one

1-(4-(3-(4-hydroxy-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)-3,3-dimethylbutan-2-one

trifluoromethylsulfonic anhydride

Downstream raw materials:

(4'-{1-ethyl-1-[4-(2-hydroxy-3,3-dimethyl-butoxy)-3-methyl-phenyl]-propyl}-3-fluoro-2'-methyl-biphenyl-4-yl)acetic acid

(4'-{1-ethyl-1-[4-(2-hydroxy-3,3-dimethyl-butoxy)-3-methyl-phenyl]-propyl}-3-fluoro-2'-methyl-biphenyl-4-yl)acetic acid

(4'-{1-ethyl-1-[4-(2-hydroxy-3,3-dimethyl-butoxy)-3-methyl-phenyl]-propyl}-3-fluoro-2'-methyl-biphenyl-4-yl)-acetic acid methyl ester

(4'-{1-ethyl-1-[4-(2-hydroxy-3,3-dimethyl-butoxy)-3-methyl-phenyl]-propyl}-3-fluoro-2'-methyl-biphenyl-4-yl)-acetic acid methyl ester

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