S-(p-bromophenyl)-S-(trifluoromethyl)-N-[(trifluoromethyl)sulfonyl]sulfoximine

Base Information

Chemical Name:S-(p-bromophenyl)-S-(trifluoromethyl)-N-[(trifluoromethyl)sulfonyl]sulfoximine
CAS No.:1421132-99-1
Molecular Formula:C₈H₄BrF₆NO₃S₂
Molecular Weight:420.151
Hs Code.:

Synonyms:S-(p-bromophenyl)-S-(trifluoromethyl)-N-[(trifluoromethyl)sulfonyl]sulfoximine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of S-(p-bromophenyl)-S-(trifluoromethyl)-N-[(trifluoromethyl)sulfonyl]sulfoximine

Chemical Property:

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Technology Process of S-(p-bromophenyl)-S-(trifluoromethyl)-N-[(trifluoromethyl)sulfonyl]sulfoximine

There total 2 articles about S-(p-bromophenyl)-S-(trifluoromethyl)-N-[(trifluoromethyl)sulfonyl]sulfoximine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1421133-03-0
(4-bromophenyl)(imino)(trifluoromethyl)-λ⁶-sulfanone

: 1421132-99-1
S-(p-bromophenyl)-S-(trifluoromethyl)-N-[(trifluoromethyl)sulfonyl]sulfoximine

Guidance literature:: (4-bromophenyl)(imino)(trifluoromethyl)-λ⁶-sulfanone; With sodium hydride; In diethyl ether; mineral oil; at 20 ℃; for 2h; Inert atmosphere;

trifluoromethylsulfonic anhydride; In dichloromethane; at -10 - 40 ℃; for 15h; Inert atmosphere;
DOI:10.1002/chem.201103460

Reference yield:

: 1178899-26-7
N-acetyl-S-(p-bromophenyl)-S-(trifluoromethyl)sulfilimine

: 1421132-99-1
S-(p-bromophenyl)-S-(trifluoromethyl)-N-[(trifluoromethyl)sulfonyl]sulfoximine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide; potassium permanganate / water / 2 h / Inert atmosphere

2.1: sodium hydride / diethyl ether; mineral oil / 2 h / 20 °C / Inert atmosphere

2.2: 15 h / -10 - 40 °C / Inert atmosphere

With potassium permanganate; sodium hydride; sodium hydroxide; In diethyl ether; water; mineral oil;
DOI:10.1002/chem.201103460

Reference yield: 48.0%

: 1421132-99-1
S-(p-bromophenyl)-S-(trifluoromethyl)-N-[(trifluoromethyl)sulfonyl]sulfoximine

: 189178-09-4
tri(4-ethynylphenyl)amine

: 1421132-95-7
tris{4-[(4-{S-(trifluoromethyl)-N-[(trifluoromethyl)sulfonyl]sulfonimidoyl}phenyl)ethynyl]phenyl}amine

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; triethylamine; triphenylphosphine; In toluene; at 40 ℃; for 5h; Inert atmosphere;
DOI:10.1002/chem.201103460