4-PHENYLENEDIGLYOXAL DIHYDRATE

Base Information

• Chemical Name: 4-PHENYLENEDIGLYOXAL DIHYDRATE
• CAS No.: 48160-61-8
• Molecular Formula: C10H10O6
• Molecular Weight: 226.18
• Hs Code.: 2914400090
• Mol file: 48160-61-8.mol

Synonyms:4-PHENYLENEDIGLYOXAL DIHYDRATE;4-Phenylenediglyoxal dihydrate 95%;4-PHENYLENEDIGLYOXAL DIHYDRATE, 95+%;Zinc02529155;1,1-(1,4-Phenylene)bis(2,2-dihydroxyethanone)

Chemical Property of 4-PHENYLENEDIGLYOXAL DIHYDRATE

Chemical Property:

• Boiling Point: 486.7 °C at 760 mmHg
• PKA: 9.97±0.41(Predicted)
• Flash Point: 248.1 °C
• PSA: 86.74000
• Density: 1.578±0.06 g/cm3(Predicted)
• LogP: 0.32120
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

4-Phenylenediglyoxal dihydrate 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-PHENYLENEDIGLYOXAL DIHYDRATE

There total 1 articles about 4-PHENYLENEDIGLYOXAL DIHYDRATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

1,4-Diacetylbenzene (1009-61-6) → 1,1'-(1,4-phenylene)bis(2,2-dihydroxyethanone) (48160-61-8)

Guidance literature:

With selenium(IV) oxide; water; In 1,4-dioxane; for 14h; Reagent/catalyst; Reflux;

DOI:10.1515/hc-2018-0039

Reference yield: 95.0%

6-amino-1-methyluracil (2434-53-9) + 1,1'-(1,4-phenylene)bis(2,2-dihydroxyethanone) (48160-61-8) + dimedone (126-81-8) → 6,6'-(1,4-phenylene)bis(5-(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-en-1-yl)-1-methyl-1,7-dihydro-2H-pyrrolo[2,3-d]pyrimidine-2,4(3H)-dione)

Guidance literature:

With tetra-n-propylammonium bromide; In ethanol; for 1.58333h; Reflux;

DOI:10.1002/jhet.3320

Reference yield: 94.0%

6-Amino-2-thiouracil (1004-40-6) + 1,1'-(1,4-phenylene)bis(2,2-dihydroxyethanone) (48160-61-8) + dimedone (126-81-8) → 5-(4,4-dimethyl-2,6-dioxocyclohexyl)-6-(4-(5-(4,4-dimethyl-2,6-dioxocyclohexyl)-4-oxo-2-thioxo-2,3,4,7-tetrahydro-1H-pyrrolo[2,3-d]pyrimidin-6-yl)phenyl)-1,7-dihydro-2H-pyrrolo[2,3-d]pyrimidine-2,4(3H)-dione

Guidance literature:

With tetra-n-propylammonium bromide; In ethanol; for 1.48333h; Reflux;

DOI:10.1002/jhet.3320

upstream raw materials:

1,4-Diacetylbenzene

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