[2-(N'-benzoyl-hydrazino)-1-benzyl-2-oxo-ethyl]-carbamic acid tert-butyl ester

Base Information

Chemical Name:[2-(N'-benzoyl-hydrazino)-1-benzyl-2-oxo-ethyl]-carbamic acid tert-butyl ester
CAS No.:888019-69-0
Molecular Formula:C₂₁H₂₅N₃O₄
Molecular Weight:383.447
Hs Code.:

Synonyms:[2-(N'-benzoyl-hydrazino)-1-benzyl-2-oxo-ethyl]-carbamic acid tert-butyl ester

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Chemical Property of [2-(N'-benzoyl-hydrazino)-1-benzyl-2-oxo-ethyl]-carbamic acid tert-butyl ester

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Technology Process of [2-(N'-benzoyl-hydrazino)-1-benzyl-2-oxo-ethyl]-carbamic acid tert-butyl ester

There total 3 articles about [2-(N'-benzoyl-hydrazino)-1-benzyl-2-oxo-ethyl]-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 1452-58-0
benzoic hydrazide hydrochloride

: 888019-69-0
[2-(N'-benzoyl-hydrazino)-1-benzyl-2-oxo-ethyl]-carbamic acid tert-butyl ester

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; for 16h;
DOI:10.1039/b916188k

Reference yield: 81.0%

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 613-94-5
benzoic acid hydrazide

: 888019-69-0
[2-(N'-benzoyl-hydrazino)-1-benzyl-2-oxo-ethyl]-carbamic acid tert-butyl ester

Guidance literature:: With triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.3390/10091218

Reference yield:

: 93-58-3,5705-52-2,80226-58-0
benzoic acid methyl ester

: 888019-69-0
[2-(N'-benzoyl-hydrazino)-1-benzyl-2-oxo-ethyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NH₂NH₂ / ethanol

2: 81 percent / HATU; Et₃N / dimethylformamide / 20 °C

With triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; hydrazine; In ethanol; N,N-dimethyl-formamide;
DOI:10.3390/10091218