(S)-(+)-4-(1-methylheptyloxycarbonyl)phenyl 4-(3-hydroxyprop-1-oxy)biphenyl-4'-carboxylate

Base Information

Chemical Name:(S)-(+)-4-(1-methylheptyloxycarbonyl)phenyl 4-(3-hydroxyprop-1-oxy)biphenyl-4'-carboxylate
CAS No.:215929-82-1
Molecular Formula:C₃₁H₃₆O₆
Molecular Weight:504.623
Hs Code.:

Synonyms:(S)-(+)-4-(1-methylheptyloxycarbonyl)phenyl 4-(3-hydroxyprop-1-oxy)biphenyl-4'-carboxylate

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Chemical Property of (S)-(+)-4-(1-methylheptyloxycarbonyl)phenyl 4-(3-hydroxyprop-1-oxy)biphenyl-4'-carboxylate

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Technology Process of (S)-(+)-4-(1-methylheptyloxycarbonyl)phenyl 4-(3-hydroxyprop-1-oxy)biphenyl-4'-carboxylate

There total 13 articles about (S)-(+)-4-(1-methylheptyloxycarbonyl)phenyl 4-(3-hydroxyprop-1-oxy)biphenyl-4'-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 215929-81-0
(S)-(+)-4-(1-methylheptyloxycarbonyl)phenyl 4-(3-benzyloxyprop-1-oxy)biphenyl-4'-carboxylate

: 215929-82-1
(S)-(+)-4-(1-methylheptyloxycarbonyl)phenyl 4-(3-hydroxyprop-1-oxy)biphenyl-4'-carboxylate

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran;

Reference yield:

: 1486-51-7
p-(benzyloxy)benzoic acid

: 215929-82-1
(S)-(+)-4-(1-methylheptyloxycarbonyl)phenyl 4-(3-hydroxyprop-1-oxy)biphenyl-4'-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: oxalyl chloride; N,N-dimethylformamide / toluene / 40 - 45 °C

2: 30.9 g / 4-dimethylaminopyridine; pyridine / toluene / 16 h / 40 - 45 °C

3: 94 percent / H₂ / Pd/C / tetrahydrofuran

4: 4-dimethylaminopyridine; pyridine / toluene / 16 h / 40 - 45 °C

5: 65 percent / H₂ / Pd/C / tetrahydrofuran

With pyridine; dmap; oxalyl dichloride; hydrogen; N,N-dimethyl-formamide; palladium on activated charcoal; In tetrahydrofuran; toluene;

Reference yield:

: 111153-21-0
4-hydroxybenzoic acid (S)-1-methylheptyl ester

: 215929-82-1
(S)-(+)-4-(1-methylheptyloxycarbonyl)phenyl 4-(3-hydroxyprop-1-oxy)biphenyl-4'-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 4-dimethylaminopyridine; pyridine / toluene / 16 h / 40 - 45 °C

2: 65 percent / H₂ / Pd/C / tetrahydrofuran

With pyridine; dmap; hydrogen; palladium on activated charcoal; In tetrahydrofuran; toluene;