4-(2-Aminoethoxy)-1-nitrobenzene hydrochloride

Base Information

• Chemical Name: 4-(2-Aminoethoxy)-1-nitrobenzene hydrochloride
• CAS No.: 98395-62-1
• Molecular Formula: C8H10 N2 O3 . Cl H
• Molecular Weight: 218.63754
• Hs Code.: 2922299090
• Mol file: 98395-62-1.mol

Synonyms:Ethanamine,2-(4-nitrophenoxy)-, monohydrochloride (9CI)

Chemical Property of 4-(2-Aminoethoxy)-1-nitrobenzene hydrochloride

Chemical Property:

• Vapor Pressure: 6.81E-06mmHg at 25°C
• Boiling Point: 371.9°Cat760mmHg
• Flash Point: 178.7°C
• PSA: 81.07000
• Density: g/cm³
• LogP: 2.95780
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

2-(4-Nitrophenoxy)ethanamineHydrochloride ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(2-Aminoethoxy)-1-nitrobenzene hydrochloride

There total 4 articles about 4-(2-Aminoethoxy)-1-nitrobenzene hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

N-(2-(4-nitrophenoxy)ethyl)phthalimide (98395-61-0) → 1-amino-2-(4-nitrophenoxy)ethane hydrochloride (98395-62-1)

Guidance literature:

With hydrogenchloride; In acetic acid; for 16h; Heating;

DOI:10.1021/jo00223a016

Reference yield:

4-nitrophenoxyethyl 4-toluenesulfonate (22483-44-9) → 1-amino-2-(4-nitrophenoxy)ethane hydrochloride (98395-62-1)

Guidance literature:

With hydrogenchloride; acetic acid; In water; Heating;

DOI:10.1021/ja00534a055

Reference yield:

2-(4-nitrophenoxy)ethanol (16365-27-8) → 1-amino-2-(4-nitrophenoxy)ethane hydrochloride (98395-62-1)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine

2: hydrochloric acid, acetic acid / H₂O / Heating

With pyridine; hydrogenchloride; acetic acid; In water;

DOI:10.1021/ja00534a055

upstream raw materials:

4-nitrophenoxyethyl 4-toluenesulfonate

N-(2-(4-nitrophenoxy)ethyl)phthalimide

2-(4-nitrophenoxy)ethanol

4-nitrophenol sodium salt

Downstream raw materials:

N-(2-hydroxyethyl)-4-nitroaniline

N-(2-hydroxyethyl)-2-hydroxy-5-nitroaniline

6-nitro-1,4-benzoxazine

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