C₃₀H₃₂

Base Information

• Chemical Name: C₃₀H₃₂
• CAS No.: 1341128-22-0
• Molecular Formula: C₃₀H₃₂
• Molecular Weight: 392.584
• Mol file: 1341128-22-0.mol

Synonyms:C₃₀H₃₂

Chemical Property of C₃₀H₃₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₃₂

There total 3 articles about C₃₀H₃₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

2-bromonaphthalen-1-yl trifluoromethanesulfonate (138719-97-8) + p-tert-butylphenylboronic acid (123324-71-0) → C30H32 (1341128-22-0)

Guidance literature:

With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; at 110 ℃; for 4h; chemoselective reaction;

DOI:10.1055/s-0030-1260955

Reference yield:

2-bromo-1-naphthol (771-15-3) → C30H32 (1341128-22-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: pyridine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C

2.1: potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 4 h / 110 °C

With pyridine; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; dichloromethane; 2.1: Suzuki- Miyaura reaction;

DOI:10.1055/s-0030-1260955

Reference yield:

3,4-dihydronaphthalene-1(2H)-one (529-34-0) → C30H32 (1341128-22-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide; dibenzoyl peroxide / benzene / 4 h / Inert atmosphere; Reflux

2.1: pyridine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C

3.1: potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 4 h / 110 °C

With pyridine; potassium phosphate; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dibenzoyl peroxide; In 1,4-dioxane; dichloromethane; benzene; 3.1: Suzuki- Miyaura reaction;

DOI:10.1055/s-0030-1260955

upstream raw materials:

2-bromo-1-naphthol

2-bromonaphthalen-1-yl trifluoromethanesulfonate

p-tert-butylphenylboronic acid

3,4-dihydronaphthalene-1(2H)-one