C₄₈H₄₆N₂O₆S₄

Base Information

Chemical Name:C₄₈H₄₆N₂O₆S₄
CAS No.:1383942-56-0
Molecular Formula:C₄₈H₄₆N₂O₆S₄
Molecular Weight:875.167
Hs Code.:

C<sub>48</sub>H<sub>46</sub>N<sub>2</sub>O<sub>6</sub>S<sub>4</sub>

Synonyms:C₄₈H₄₆N₂O₆S₄

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Chemical Property of C₄₈H₄₆N₂O₆S₄

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Technology Process of C₄₈H₄₆N₂O₆S₄

There total 3 articles about C₄₈H₄₆N₂O₆S₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1383942-49-1
C₄₅H₄₅NO₅S₄

: 372-09-8
cyanoacetic acid

: 1383942-56-0
C₄₈H₄₆N₂O₆S₄

Guidance literature:: With piperidine; acetic acid; In chloroform; for 12h; Reflux;
DOI:10.1016/j.tet.2012.04.113

Reference yield:

: 175922-79-9
tributyl(2,3-dihydrothieno[3,4-b][1,4]dioxin-5-yl)-stannane

: 1383942-56-0
C₄₈H₄₆N₂O₆S₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / para-xylene / 5 h / Inert atmosphere; Reflux

2.1: trichlorophosphate / 1 h / 0 °C

2.2: 1 h / 0 - 20 °C

2.3: pH 10

3.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 20 °C

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / para-xylene / 24 h / Inert atmosphere; Reflux

5.1: piperidine; acetic acid / chloroform / 12 h / Reflux

With piperidine; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; acetic acid; trichlorophosphate; In chloroform; para-xylene; N,N-dimethyl-formamide; 1.1: Stille coupling / 2.2: Vilsmeier-Haack reaction / 4.1: Stille coupling / 5.1: Knoevenagel condensation;
DOI:10.1016/j.tet.2012.04.113

Reference yield:

: 1383942-36-6
C₁₄H₈O₂S₄

: 1383942-56-0
C₄₈H₄₆N₂O₆S₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: trichlorophosphate / 1 h / 0 °C

1.2: 1 h / 0 - 20 °C

1.3: pH 10

2.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 20 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / para-xylene / 24 h / Inert atmosphere; Reflux

4.1: piperidine; acetic acid / chloroform / 12 h / Reflux

With piperidine; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; acetic acid; trichlorophosphate; In chloroform; para-xylene; N,N-dimethyl-formamide; 1.2: Vilsmeier-Haack reaction / 3.1: Stille coupling / 4.1: Knoevenagel condensation;
DOI:10.1016/j.tet.2012.04.113