methyl 3-azido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-2-fluoro-α-D-gulopyranoside

Base Information

Chemical Name:methyl 3-azido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-2-fluoro-α-D-gulopyranoside
CAS No.:105600-38-2
Molecular Formula:C₁₄H₁₅BrFN₃O₄
Molecular Weight:388.193
Hs Code.:

Synonyms:methyl 3-azido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-2-fluoro-α-D-gulopyranoside

Suppliers and Price of methyl 3-azido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-2-fluoro-α-D-gulopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 3-azido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-2-fluoro-α-D-gulopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 3-azido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-2-fluoro-α-D-gulopyranoside

There total 3 articles about methyl 3-azido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-2-fluoro-α-D-gulopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 105600-37-1
methyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-α-D-gulopyranoside

: 105600-38-2
methyl 3-azido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-2-fluoro-α-D-gulopyranoside

Guidance literature:: With N-Bromosuccinimide; barium carbonate; In tetrachloromethane; for 1h; Heating;
DOI:10.1016/S0008-6215(00)90313-6

Reference yield:

: 3673-00-5
methyl 3-azido-4,6-O-benzylidene-3-deoxy-α-D-idopyranoside

: 105600-38-2
methyl 3-azido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-2-fluoro-α-D-gulopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / pyridine / 2 h / 0 °C

2: 78 percent / tetrabutylammonium fluoride / dimethylformamide / 5 h / Ambient temperature

3: 56 percent / N-bromosuccinimide, BaCO₃ / CCl₄ / 1 h / Heating

With pyridine; N-Bromosuccinimide; tetrabutyl ammonium fluoride; barium carbonate; In tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)90313-6

Reference yield:

: 105600-36-0
methyl 3-azido-4,6-O-benzylidene-3-deoxy-2-O-trifluoromethanesulphonyl-α-D-idopyranoside

: 105600-38-2
methyl 3-azido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-2-fluoro-α-D-gulopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / tetrabutylammonium fluoride / dimethylformamide / 5 h / Ambient temperature

2: 56 percent / N-bromosuccinimide, BaCO₃ / CCl₄ / 1 h / Heating

With N-Bromosuccinimide; tetrabutyl ammonium fluoride; barium carbonate; In tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)90313-6