4'-<<2-n-butyl-6-(butanesultam-1-yl)benzimidazol-1-yl>methyl>-2-cyanobiphenyl

Base Information

Chemical Name:4'-<<2-n-butyl-6-(butanesultam-1-yl)benzimidazol-1-yl>methyl>-2-cyanobiphenyl
CAS No.:141864-93-9
Molecular Formula:C₂₉H₃₀N₄O₂S
Molecular Weight:498.649
Hs Code.:

Synonyms:4'-<<2-n-butyl-6-(butanesultam-1-yl)benzimidazol-1-yl>methyl>-2-cyanobiphenyl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4'-<<2-n-butyl-6-(butanesultam-1-yl)benzimidazol-1-yl>methyl>-2-cyanobiphenyl

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Technology Process of 4'-<<2-n-butyl-6-(butanesultam-1-yl)benzimidazol-1-yl>methyl>-2-cyanobiphenyl

There total 6 articles about 4'-<<2-n-butyl-6-(butanesultam-1-yl)benzimidazol-1-yl>methyl>-2-cyanobiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1027567-23-2
4-Chloro-butane-1-sulfonic acid [2-butyl-3-(2'-cyano-biphenyl-4-ylmethyl)-3H-benzoimidazol-5-yl]-amide

: 141864-93-9
4'-<<2-n-butyl-6-(butanesultam-1-yl)benzimidazol-1-yl>methyl>-2-cyanobiphenyl

Guidance literature:: With sodium ethanolate; In ethanol; for 1h; Yield given; Heating;
DOI:10.1021/jm00077a007

Reference yield:

: 114772-54-2
4'-(bromomethyl)-1,1'-biphenyl-2-carbonitrile

: 141864-93-9
4'-<<2-n-butyl-6-(butanesultam-1-yl)benzimidazol-1-yl>methyl>-2-cyanobiphenyl

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) t-BuOK, 3.) H₂, Raney nickel

2: Et₃N / tetrahydrofuran / 5 h / Ambient temperature

3: EtONa / ethanol / 1 h / Heating

With potassium tert-butylate; hydrogen; sodium ethanolate; nickel; triethylamine; In tetrahydrofuran; ethanol;
DOI:10.1021/jm00077a007

Reference yield:

: 99-56-9
4-Nitrophenylene-1,2-diamine

: 141864-93-9
4'-<<2-n-butyl-6-(butanesultam-1-yl)benzimidazol-1-yl>methyl>-2-cyanobiphenyl

Guidance literature:: Multi-step reaction with 4 steps

1: 62 percent / POCl₃ / 3 h / Heating

2: 1.) t-BuOK, 3.) H₂, Raney nickel

3: Et₃N / tetrahydrofuran / 5 h / Ambient temperature

4: EtONa / ethanol / 1 h / Heating

With potassium tert-butylate; hydrogen; sodium ethanolate; nickel; triethylamine; trichlorophosphate; In tetrahydrofuran; ethanol;
DOI:10.1021/jm00077a007