2-[4-(4-bromobutoxy)phenyl]-5-dodecylpyrimidine

Base Information

Chemical Name:2-[4-(4-bromobutoxy)phenyl]-5-dodecylpyrimidine
CAS No.:1403575-04-1
Molecular Formula:C₂₆H₃₉BrN₂O
Molecular Weight:475.512
Hs Code.:

Synonyms:2-[4-(4-bromobutoxy)phenyl]-5-dodecylpyrimidine

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Chemical Property of 2-[4-(4-bromobutoxy)phenyl]-5-dodecylpyrimidine

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Technology Process of 2-[4-(4-bromobutoxy)phenyl]-5-dodecylpyrimidine

There total 4 articles about 2-[4-(4-bromobutoxy)phenyl]-5-dodecylpyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 110-52-1
1,4-dibromo-butane

: 102408-55-9
5-n-dodecyl-2-(4-hydroxyphenyl)pyrimidine

: 1403575-04-1
2-[4-(4-bromobutoxy)phenyl]-5-dodecylpyrimidine

Guidance literature:: 5-n-dodecyl-2-(4-hydroxyphenyl)pyrimidine; With potassium hydroxide; In dimethyl sulfoxide; at 20 ℃; for 0.166667h; Inert atmosphere;

1,4-dibromo-butane; In dimethyl sulfoxide; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c2jm34595a

Reference yield:

: 14620-53-2
1,1-dimethoxytetradecane

: 1403575-04-1
2-[4-(4-bromobutoxy)phenyl]-5-dodecylpyrimidine

Guidance literature:: Multi-step reaction with 3 steps

1.1: trichlorophosphate / 40 °C / Inert atmosphere; Cooling with ice

1.2: 2 h / 40 - 60 °C / Inert atmosphere

2.1: sodium methylate / methanol / 14 h / 20 °C / Inert atmosphere; Reflux

3.1: potassium hydroxide / dimethyl sulfoxide / 0.17 h / 20 °C / Inert atmosphere

3.2: 12 h / 20 °C / Inert atmosphere

With sodium methylate; potassium hydroxide; trichlorophosphate; In methanol; dimethyl sulfoxide;
DOI:10.1039/c2jm34595a

Reference yield:

: 38148-63-9
p-amidinophenol hydrochloride

: 1403575-04-1
2-[4-(4-bromobutoxy)phenyl]-5-dodecylpyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium methylate / methanol / 14 h / 20 °C / Inert atmosphere; Reflux

2.1: potassium hydroxide / dimethyl sulfoxide / 0.17 h / 20 °C / Inert atmosphere

2.2: 12 h / 20 °C / Inert atmosphere

With sodium methylate; potassium hydroxide; In methanol; dimethyl sulfoxide;
DOI:10.1039/c2jm34595a