Tetradecanal dimethyl acetal

Base Information

Chemical Name:Tetradecanal dimethyl acetal
CAS No.:14620-53-2
Molecular Formula:C16H34O2
Molecular Weight:258.44000
Hs Code.:
Mol file:14620-53-2.mol

Synonyms:Myristinaldehyd-dimethylacetal;myristaldehyde dimethyl acetal;1,1-Dimethoxy-tetradecan;1,1-Dimethoxy-tetradecane;Tetradecane, 1,1-dimethoxy-;

Suppliers and Price of Tetradecanal dimethyl acetal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of Tetradecanal dimethyl acetal

Chemical Property:

Refractive Index:1.4342 (estimate)
Boiling Point:134 - 136 °C (4 mmHg)
PSA：18.46000
Density:0.9581 (rough estimate)
LogP:5.30640

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Tetradecanal dimethyl acetal

There total 2 articles about Tetradecanal dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 67-56-1
methanol

: 124-25-4,511542-15-7
myristylaldehyde

: 14620-53-2
1,1-dimethoxytetradecane

Guidance literature:: aminopropylated Silica-Gel hydrochloride (APSG*HCl) resin; for 10h; Ambient temperature;
DOI:10.1016/S0040-4020(01)91796-X

Reference yield:

: 14620-53-2
1,1-dimethoxytetradecane

Guidance literature:: DOI:10.1039/j39680002030

Reference yield:

: 14620-53-2
1,1-dimethoxytetradecane

: 1402081-73-5
((2R,3S,4R,5R,6R)-3-(benzyloxy)-6-((R)-4-ethyl-2-oxooxazolidin-3-yl)-5-hexyl-4-tridecyltetrahydro-2H-pyran-2-yl)methyl pivalate

Guidance literature:: Multi-step reaction with 7 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 3 h / -78 - 0 °C / Inert atmosphere

2.1: silica gel / toluene / 0.5 h / 110 °C / Inert atmosphere

3.1: tris(6,6,7,7,8,8-heptafluoro-2,2-dimethyl-3,5-octadionato)europium(III) / cyclohexane / 24 h / 80 °C / Inert atmosphere

4.1: boron trifluoride diethyl etherate; diisobutylaluminium hydride / dichloromethane; toluene / 4 h / -78 - 20 °C / Inert atmosphere

5.1: dimethylsulfide borane complex / tetrahydrofuran / 25.5 h / 0 - 20 °C / Inert atmosphere

5.2: 1.5 h / Inert atmosphere; Reflux

6.1: pyridine / dichloromethane / 17 h / 0 - 20 °C / Inert atmosphere

7.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 17 h / -15 - 20 °C / Inert atmosphere

With pyridine; tris(6,6,7,7,8,8-heptafluoro-2,2-dimethyl-3,5-octadionato)europium(III); dimethylsulfide borane complex; boron trifluoride diethyl etherate; silica gel; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; dichloromethane; cyclohexane; N,N-dimethyl-formamide; toluene; mineral oil; 3.1: Diels-Alder reaction;
DOI:10.1002/ejoc.201200513