1-(1-benzyl-1H-tetrazol-5-yl)-2-bromoethanone oxime

Base Information

Chemical Name:1-(1-benzyl-1H-tetrazol-5-yl)-2-bromoethanone oxime
CAS No.:1343478-79-4
Molecular Formula:C₁₀H₁₀BrN₅O
Molecular Weight:296.126
Hs Code.:

Synonyms:1-(1-benzyl-1H-tetrazol-5-yl)-2-bromoethanone oxime

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Chemical Property of 1-(1-benzyl-1H-tetrazol-5-yl)-2-bromoethanone oxime

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Technology Process of 1-(1-benzyl-1H-tetrazol-5-yl)-2-bromoethanone oxime

There total 3 articles about 1-(1-benzyl-1H-tetrazol-5-yl)-2-bromoethanone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1343478-77-2
1-(1-benzyl-1H-tetrazol-5-yl)-2-bromoethanone

: 1343478-79-4
1-(1-benzyl-1H-tetrazol-5-yl)-2-bromoethanone oxime

Guidance literature:: With hydroxylamine hydrochloride; In methanol; dichloromethane; at 20 ℃; for 72h;
DOI:10.1016/j.tet.2011.09.051

Reference yield:

: 120869-86-5
5-acetyl-1-benzyl-1H-tetrazole

: 1343478-79-4
1-(1-benzyl-1H-tetrazol-5-yl)-2-bromoethanone oxime

Guidance literature:: Multi-step reaction with 2 steps

1: 1,4-dioxane; bromine / diethyl ether / 19 h / 20 °C

2: hydroxylamine hydrochloride / methanol; dichloromethane / 72 h / 20 °C

With 1,4-dioxane; hydroxylamine hydrochloride; bromine; In methanol; diethyl ether; dichloromethane;
DOI:10.1016/j.tet.2011.09.051

Reference yield:

: 622-79-7
benzyl azide

: 1343478-79-4
1-(1-benzyl-1H-tetrazol-5-yl)-2-bromoethanone oxime

Guidance literature:: Multi-step reaction with 3 steps

1: 24 h / 120 °C / Sealed vessel; Neat (no solvent)

2: 1,4-dioxane; bromine / diethyl ether / 19 h / 20 °C

3: hydroxylamine hydrochloride / methanol; dichloromethane / 72 h / 20 °C

With 1,4-dioxane; hydroxylamine hydrochloride; bromine; In methanol; diethyl ether; dichloromethane;
DOI:10.1016/j.tet.2011.09.051