3-Pyrimidin-2-ylbenzyl chloride

Base Information

• Chemical Name: 3-Pyrimidin-2-ylbenzyl chloride
• CAS No.: 898289-51-5
• Molecular Formula: C₁₁H₉ClN₂
• Molecular Weight: 204.659
• Hs Code.: 2933599090
• Mol file: 898289-51-5.mol

Synonyms:3-(Pyrimidin-2-yl)benzyl chloride 97%;

Chemical Property of 3-Pyrimidin-2-ylbenzyl chloride

Chemical Property:

• Vapor Pressure: 0.0128mmHg at 25°C
• Melting Point: 68-70 °C
• Refractive Index: 1.587
• Boiling Point: 268.3 °C at 760 mmHg
• Flash Point: 142 °C
• PSA: 25.78000
• Density: 1.212 g/cm³
• LogP: 2.88240
• Storage Temp.: -20°C Freezer
• Solubility.: Acetonitrile (Slightly), Chloroform (Slightly)

Purity/Quality:

99% ^*data from raw suppliers

2-[3-(Chloromethyl)phenyl]pyrimidine ^*data from reagent suppliers

Safty Information:

• Pictogram(s): C
• Hazard Codes: C

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2-[3-(Chloromethyl)phenyl]pyrimidine is useful in the preparation of formyl arenes.

Technology Process of 3-Pyrimidin-2-ylbenzyl chloride

There total 1 articles about 3-Pyrimidin-2-ylbenzyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-phenylpyrimidine (7431-45-0) → 2-(3-(chloromethyl)phenyl)pyrimidine (898289-51-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: potassium carbonate; N-Ac-Leu; [Ru(OAc)2(p-cymene)] / acetonitrile / 24 h / 120 °C / Sealed tube; Inert atmosphere

2.1: sodium tetrahydroborate / methanol / 12 h / 20 °C

2.2: Reflux

With sodium tetrahydroborate; N-Ac-Leu; [Ru(OAc)2(p-cymene)]; potassium carbonate; In methanol; acetonitrile;

DOI:10.1021/acs.joc.0c00007

upstream raw materials:

2-phenylpyrimidine

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