9-[(9H-4,5-Diazafluoren-9-ylidene)-2,5-dimethylphenylmethyl]-9H-4,5-diazafluorene

Base Information

Chemical Name:9-[(9H-4,5-Diazafluoren-9-ylidene)-2,5-dimethylphenylmethyl]-9H-4,5-diazafluorene
CAS No.:272458-08-9
Molecular Formula:C₃₁H₂₂N₄
Molecular Weight:450.542
Hs Code.:

Synonyms:9-[(9H-4,5-Diazafluoren-9-ylidene)-2,5-dimethylphenylmethyl]-9H-4,5-diazafluorene

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Chemical Property of 9-[(9H-4,5-Diazafluoren-9-ylidene)-2,5-dimethylphenylmethyl]-9H-4,5-diazafluorene

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Technology Process of 9-[(9H-4,5-Diazafluoren-9-ylidene)-2,5-dimethylphenylmethyl]-9H-4,5-diazafluorene

There total 3 articles about 9-[(9H-4,5-Diazafluoren-9-ylidene)-2,5-dimethylphenylmethyl]-9H-4,5-diazafluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 245-37-4
4,5-diazafluorene

: 272458-07-8
(9H-4,5-Diazafluoren-9-ylidene)-2,5-dimethylphenylmethane

: 272458-08-9
9-[(9H-4,5-Diazafluoren-9-ylidene)-2,5-dimethylphenylmethyl]-9H-4,5-diazafluorene

Guidance literature:: With air; potassium tert-butylate; In N,N-dimethyl-formamide; at 20 ℃; for 4h;

Reference yield:

: 50890-67-0
4,5-Diazafluoren-9-one

: 272458-08-9
9-[(9H-4,5-Diazafluoren-9-ylidene)-2,5-dimethylphenylmethyl]-9H-4,5-diazafluorene

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / NH₂NH₂*H₂O / 6 h / 180 °C

2: 95 percent / KOH / phenylmethanol / 48 h / 40 °C

3: 20 percent / t-BuOK; air / dimethylformamide / 4 h / 20 °C

With potassium hydroxide; air; potassium tert-butylate; hydrazine hydrate; In N,N-dimethyl-formamide; benzyl alcohol; 1: Reduction / 2: Condensation / 3: Alkylation;

Reference yield:

: 245-37-4
4,5-diazafluorene

: 272458-08-9
9-[(9H-4,5-Diazafluoren-9-ylidene)-2,5-dimethylphenylmethyl]-9H-4,5-diazafluorene

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / KOH / phenylmethanol / 48 h / 40 °C

2: 20 percent / t-BuOK; air / dimethylformamide / 4 h / 20 °C

With potassium hydroxide; air; potassium tert-butylate; In N,N-dimethyl-formamide; benzyl alcohol; 1: Condensation / 2: Alkylation;