methyl (S)-2-<2-{N-[1-phenyl-2-(triisopropylsilyloxy)ethyl]carbamoylmethyl}phenyl>acetate

Base Information

Chemical Name:methyl (S)-2-<2-{N-[1-phenyl-2-(triisopropylsilyloxy)ethyl]carbamoylmethyl}phenyl>acetate
CAS No.:929297-11-0
Molecular Formula:C₂₈H₄₁NO₄Si
Molecular Weight:483.723
Hs Code.:

Synonyms:methyl (S)-2-<2-{N-[1-phenyl-2-(triisopropylsilyloxy)ethyl]carbamoylmethyl}phenyl>acetate

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Chemical Property of methyl (S)-2-<2-{N-[1-phenyl-2-(triisopropylsilyloxy)ethyl]carbamoylmethyl}phenyl>acetate

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Technology Process of methyl (S)-2-<2-{N-[1-phenyl-2-(triisopropylsilyloxy)ethyl]carbamoylmethyl}phenyl>acetate

There total 4 articles about methyl (S)-2-<2-{N-[1-phenyl-2-(triisopropylsilyloxy)ethyl]carbamoylmethyl}phenyl>acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 929297-10-9
methyl (S)-2-{2-[N-(2-hydroxy-1-phenylethyl)carbamoylmethyl]phenyl}acetate

: 13154-24-0
triisopropylsilyl chloride

: 929297-11-0
methyl (S)-2-<2-{N-[1-phenyl-2-(triisopropylsilyloxy)ethyl]carbamoylmethyl}phenyl>acetate

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1002/ejoc.200600746

Reference yield:

: 929297-09-6
(S)-2-{[N-(2-hydroxy-1-phenylethyl)carbamoylmethyl]phenyl}acetic acid

: 929297-11-0
methyl (S)-2-<2-{N-[1-phenyl-2-(triisopropylsilyloxy)ethyl]carbamoylmethyl}phenyl>acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / methanol / 19 h / 20 °C

2: 85 percent / imidazole / dimethylformamide / 16 h / 20 °C

With 1H-imidazole; In methanol; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200600746

Reference yield:

: 7500-53-0
1,2-Phenylenediacetic acid

: 929297-11-0
methyl (S)-2-<2-{N-[1-phenyl-2-(triisopropylsilyloxy)ethyl]carbamoylmethyl}phenyl>acetate

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent Spectr_. / thionyl chloride / toluene / 24 h / Heating

2: 54 percent / triethylamine / CH₂Cl₂ / 3 h / 20 °C

3: 58 percent / methanol / 19 h / 20 °C

4: 85 percent / imidazole / dimethylformamide / 16 h / 20 °C

With 1H-imidazole; thionyl chloride; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/ejoc.200600746