1-{2,4-bis(benzyloxy)-6-(tert-butyldiphenylsilyloxy)-3-[(2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl]phenyl}ethanone

Base Information

• Chemical Name: 1-{2,4-bis(benzyloxy)-6-(tert-butyldiphenylsilyloxy)-3-[(2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl]phenyl}ethanone
• CAS No.: 1064179-48-1
• Molecular Formula: C₇₂H₇₂O₉Si
• Molecular Weight: 1109.44

Synonyms:1-{2,4-bis(benzyloxy)-6-(tert-butyldiphenylsilyloxy)-3-[(2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl]phenyl}ethanone

Chemical Property of 1-{2,4-bis(benzyloxy)-6-(tert-butyldiphenylsilyloxy)-3-[(2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl]phenyl}ethanone

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Technology Process of 1-{2,4-bis(benzyloxy)-6-(tert-butyldiphenylsilyloxy)-3-[(2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl]phenyl}ethanone

There total 1 articles about 1-{2,4-bis(benzyloxy)-6-(tert-butyldiphenylsilyloxy)-3-[(2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl]phenyl}ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

C65H66O9Si (1064179-44-7) + benzyl alcohol (100-51-6,185532-71-2) → 1-{2,4-bis(benzyloxy)-6-(tert-butyldiphenylsilyloxy)-3-[(2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl]phenyl}ethanone (1064179-48-1)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1021/ol900689m

Reference yield: 68.0%

(1H-benzo[d][1,2,3]triazol-1-yl)[4-(benzyloxy)phenyl]methanone (897599-06-3) + 1-{2,4-bis(benzyloxy)-6-(tert-butyldiphenylsilyloxy)-3-[(2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl]phenyl}ethanone (1064179-48-1) → 1-[4-(benzyloxy)phenyl]-3-{2,4-bis(benzyloxy)-6-(tert-butyldiphenylsilyloxy)-3-[(2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl]phenyl}propane-1,3-dione (1064179-53-8)

Guidance literature:

With potassium hexamethylsilazane; In tetrahydrofuran; at -78 ℃; for 1.5h; Inert atmosphere;

DOI:10.1021/ol900689m

upstream raw materials:

C₆₅H₆₆O₉Si

benzyl alcohol

Downstream raw materials:

1-[4-(benzyloxy)phenyl]-3-{2,4-bis(benzyloxy)-6-(tert-butyldiphenylsilyloxy)-3-[(2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl]phenyl}propane-1,3-dione

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