2-azido-3,4,6-tri-O-benzyl-2-deoxy-D-α-glucopyranosyI-(1-6)-3,4,5-tri-O-benzyl-1,2-didehydro-1,2-dideoxy-D-myo-inositol

Base Information

Chemical Name:2-azido-3,4,6-tri-O-benzyl-2-deoxy-D-α-glucopyranosyI-(1-6)-3,4,5-tri-O-benzyl-1,2-didehydro-1,2-dideoxy-D-myo-inositol
CAS No.:1035456-87-1
Molecular Formula:C₅₄H₅₅N₃O₈
Molecular Weight:874.046
Hs Code.:

Synonyms:2-azido-3,4,6-tri-O-benzyl-2-deoxy-D-α-glucopyranosyI-(1-6)-3,4,5-tri-O-benzyl-1,2-didehydro-1,2-dideoxy-D-myo-inositol

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Chemical Property of 2-azido-3,4,6-tri-O-benzyl-2-deoxy-D-α-glucopyranosyI-(1-6)-3,4,5-tri-O-benzyl-1,2-didehydro-1,2-dideoxy-D-myo-inositol

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Technology Process of 2-azido-3,4,6-tri-O-benzyl-2-deoxy-D-α-glucopyranosyI-(1-6)-3,4,5-tri-O-benzyl-1,2-didehydro-1,2-dideoxy-D-myo-inositol

There total 2 articles about 2-azido-3,4,6-tri-O-benzyl-2-deoxy-D-α-glucopyranosyI-(1-6)-3,4,5-tri-O-benzyl-1,2-didehydro-1,2-dideoxy-D-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 102997-58-0
(1R,2R,3S)-tris(phenylmethoxy)-6S-hydroxy-cyclohex-4-ene

: 220688-25-5
O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α/β-D-glucopyranosyl) trichloroacetimidate

: 1035456-87-1
2-azido-3,4,6-tri-O-benzyl-2-deoxy-D-α-glucopyranosyI-(1-6)-3,4,5-tri-O-benzyl-1,2-didehydro-1,2-dideoxy-D-myo-inositol

: 2-azido-3,4,6-tri-O-benzyl-2-deoxy-D-β-glucopyranosyI-(1-6)-3,4,5-tri-O-benzyl-1,2-didehydro-1,2-dideoxy-D-myo-inositol

Guidance literature:: (1R,2R,3S)-tris(phenylmethoxy)-6S-hydroxy-cyclohex-4-ene; O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α/β-D-glucopyranosyl) trichloroacetimidate; With molecular sieve; trifluorormethanesulfonic acid; In diethyl ether; at -5 - 20 ℃;

With sodium hydrogencarbonate; In diethyl ether; at 20 ℃; for 0.25h;

Reference yield: 17.0%

: 102997-58-0
(1R,2R,3S)-tris(phenylmethoxy)-6S-hydroxy-cyclohex-4-ene

: 220688-25-5
O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α/β-D-glucopyranosyl) trichloroacetimidate

: 1035456-87-1
2-azido-3,4,6-tri-O-benzyl-2-deoxy-D-α-glucopyranosyI-(1-6)-3,4,5-tri-O-benzyl-1,2-didehydro-1,2-dideoxy-D-myo-inositol

: 2-azido-3,4,6-tri-O-benzyl-2-deoxy-D-β-glucopyranosyI-(1-6)-3,4,5-tri-O-benzyl-1,2-didehydro-1,2-dideoxy-D-myo-inositol

: 2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl fluoride

Guidance literature:: (1R,2R,3S)-tris(phenylmethoxy)-6S-hydroxy-cyclohex-4-ene; O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α/β-D-glucopyranosyl) trichloroacetimidate; With molecular sieve; boron trifluoride diethyl etherate; In dichloromethane; at -20 ℃; for 3h;

With sodium hydrogencarbonate; In dichloromethane; at 20 ℃; for 0.25h;

Reference yield:

: 1035456-87-1
2-azido-3,4,6-tri-O-benzyl-2-deoxy-D-α-glucopyranosyI-(1-6)-3,4,5-tri-O-benzyl-1,2-didehydro-1,2-dideoxy-D-myo-inositol

: C₅₄H₅₇N₃O₁₀

: 133163-53-8
O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-1,5,6-tri-O-benzyl-L-myo-inositol

Guidance literature:: 2-azido-3,4,6-tri-O-benzyl-2-deoxy-D-α-glucopyranosyI-(1-6)-3,4,5-tri-O-benzyl-1,2-didehydro-1,2-dideoxy-D-myo-inositol; With 1,4-diaza-bicyclo[2.2.2]octane; osmium(VIII) oxide; methanesulfonamide; potassium carbonate; potassium hexacyanoferrate(III); In tetrahydrofuran; water; tert-butyl alcohol;

With sodium hydroxide; at 60 ℃;