O-benzyl-N-((2S,3S,4R)-2,3,4-tris-benzyloxy-5-triisopropylsilanyloxy-1-trityloxymethylpentyl)-hydroxylamine

Base Information

Chemical Name:O-benzyl-N-((2S,3S,4R)-2,3,4-tris-benzyloxy-5-triisopropylsilanyloxy-1-trityloxymethylpentyl)-hydroxylamine
CAS No.:1607820-97-2
Molecular Formula:C₆₂H₇₃NO₆Si
Molecular Weight:956.35
Hs Code.:

Synonyms:O-benzyl-N-((2S,3S,4R)-2,3,4-tris-benzyloxy-5-triisopropylsilanyloxy-1-trityloxymethylpentyl)-hydroxylamine

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Chemical Property of O-benzyl-N-((2S,3S,4R)-2,3,4-tris-benzyloxy-5-triisopropylsilanyloxy-1-trityloxymethylpentyl)-hydroxylamine

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Technology Process of O-benzyl-N-((2S,3S,4R)-2,3,4-tris-benzyloxy-5-triisopropylsilanyloxy-1-trityloxymethylpentyl)-hydroxylamine

There total 7 articles about O-benzyl-N-((2S,3S,4R)-2,3,4-tris-benzyloxy-5-triisopropylsilanyloxy-1-trityloxymethylpentyl)-hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1607820-93-8
triisopropyl-((2R,3S,4S)-2,3,4-trisbenzyloxyhex-5-enyloxy)silane

: 1607820-97-2
O-benzyl-N-((2S,3S,4R)-2,3,4-tris-benzyloxy-5-triisopropylsilanyloxy-1-trityloxymethylpentyl)-hydroxylamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: 4-methylmorpholine N-oxide; osmium(VIII) oxide / water; acetone; tert-butyl alcohol / 0 - 20 °C

2.1: triethylamine; dmap / tetrahydrofuran / 20 h / Inert atmosphere; Reflux

3.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 20 h / 20 °C

4.1: pyridine / methanol / 20 h / Inert atmosphere; Reflux

4.2: 1.5 h / 0 °C / Inert atmosphere

With pyridine; dmap; osmium(VIII) oxide; tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; acetone; tert-butyl alcohol;

Reference yield:

: 1607820-95-0
(3S,4R,5R)-3,4,5-trisbenzyloxy-6-triisopropylsilanyloxy-1-trityloxyhexan-2-ol

: 1607820-97-2
O-benzyl-N-((2S,3S,4R)-2,3,4-tris-benzyloxy-5-triisopropylsilanyloxy-1-trityloxymethylpentyl)-hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 20 h / 20 °C

2.1: pyridine / methanol / 20 h / Inert atmosphere; Reflux

2.2: 1.5 h / 0 °C / Inert atmosphere

With pyridine; tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In methanol; dichloromethane;

Reference yield:

: 1607820-94-9
(3S,4R,5R)-3,4,5-tris-benzyloxy-6-triisopropylsilanyloxy-hexane-1,2-diol

: 1607820-97-2
O-benzyl-N-((2S,3S,4R)-2,3,4-tris-benzyloxy-5-triisopropylsilanyloxy-1-trityloxymethylpentyl)-hydroxylamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; dmap / tetrahydrofuran / 20 h / Inert atmosphere; Reflux

2.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 20 h / 20 °C

3.1: pyridine / methanol / 20 h / Inert atmosphere; Reflux

3.2: 1.5 h / 0 °C / Inert atmosphere

With pyridine; dmap; tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane;