(2R)-2-tert-butoxycarbonylamino-3-(4'-dibenzofuran-4-yl-biphenyl-4-ylmethylsulfinyl)-propionic acid

Base Information

Chemical Name:(2R)-2-tert-butoxycarbonylamino-3-(4'-dibenzofuran-4-yl-biphenyl-4-ylmethylsulfinyl)-propionic acid
CAS No.:796071-11-9
Molecular Formula:C₃₃H₃₁NO₆S
Molecular Weight:569.678
Hs Code.:

Synonyms:(2R)-2-tert-butoxycarbonylamino-3-(4'-dibenzofuran-4-yl-biphenyl-4-ylmethylsulfinyl)-propionic acid

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Chemical Property of (2R)-2-tert-butoxycarbonylamino-3-(4'-dibenzofuran-4-yl-biphenyl-4-ylmethylsulfinyl)-propionic acid

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Technology Process of (2R)-2-tert-butoxycarbonylamino-3-(4'-dibenzofuran-4-yl-biphenyl-4-ylmethylsulfinyl)-propionic acid

There total 9 articles about (2R)-2-tert-butoxycarbonylamino-3-(4'-dibenzofuran-4-yl-biphenyl-4-ylmethylsulfinyl)-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 796070-89-8
(R)-2-tert-butoxycarbonylamino-3-(4'-dibenzofuran-4-yl-biphenyl-4-ylmethylsulfanyl)-propionic acid

: 796071-11-9
(2R)-2-tert-butoxycarbonylamino-3-(4'-dibenzofuran-4-yl-biphenyl-4-ylmethylsulfinyl)-propionic acid

Guidance literature:: With sodium perborate; In acetic acid; at 40 ℃; for 1h;

Reference yield:

: 955959-84-9
4-(4-bromophenyl)dibenzofuran

: 796071-11-9
(2R)-2-tert-butoxycarbonylamino-3-(4'-dibenzofuran-4-yl-biphenyl-4-ylmethylsulfinyl)-propionic acid

Guidance literature:: Multi-step reaction with 6 steps

1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ethanol; water; toluene / 2 - 3 h / 100 °C

2: sodium tetrahydroborate / tetrahydrofuran; ethanol / 0.08 - 0.17 h / 20 °C

3: triethylamine / dichloromethane / 2 - 4 h / 0 °C

4: caesium carbonate / DMF (N,N-dimethyl-formamide) / 2 - 3 h / 20 °C

5: sodium hydroxide; water / tetrahydrofuran; methanol / 20 °C

6: sodium perborate; acetic acid / 1 h / 40 °C

With sodium hydroxide; sodium tetrahydroborate; sodium perborate; water; sodium carbonate; caesium carbonate; acetic acid; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane; water; toluene;

Reference yield:

: 100124-06-9
4-dibenzofurylboronic acid

: 796071-11-9
(2R)-2-tert-butoxycarbonylamino-3-(4'-dibenzofuran-4-yl-biphenyl-4-ylmethylsulfinyl)-propionic acid

Guidance literature:: Multi-step reaction with 7 steps

1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ethanol; water; toluene / 2 - 3 h / 90 °C

2: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ethanol; water; toluene / 2 - 3 h / 100 °C

3: sodium tetrahydroborate / tetrahydrofuran; ethanol / 0.08 - 0.17 h / 20 °C

4: triethylamine / dichloromethane / 2 - 4 h / 0 °C

5: caesium carbonate / DMF (N,N-dimethyl-formamide) / 2 - 3 h / 20 °C

6: sodium hydroxide; water / tetrahydrofuran; methanol / 20 °C

7: sodium perborate; acetic acid / 1 h / 40 °C

With sodium hydroxide; sodium tetrahydroborate; sodium perborate; water; sodium carbonate; caesium carbonate; acetic acid; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane; water; toluene;