V(CO)5{P(C₆H₅)3}

Base Information

Chemical Name:V(CO)5{P(C₆H₅)3}
CAS No.:72622-82-3
Molecular Formula:C₂₃H₁₅O₅PV
Molecular Weight:453.284
Hs Code.:

Synonyms:V(CO)5{P(C₆H₅)3}

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of V(CO)5{P(C₆H₅)3}

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Technology Process of V(CO)5{P(C₆H₅)3}

There total 5 articles about V(CO)5{P(C₆H₅)3} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 14024-00-1
vanadium hexacarbonyl

: 72622-82-3
V(CO)5{P(C₆H₅)3}

Guidance literature:: With PPh₃; In dichloromethane; under N2 after addn. of PPh3 to V(CO)6 in CH2Cl2 at -70°C soln. stirred for 1.5 h at 0°C; hexane added, CH2Cl2 removed in vac. at 0°C, solid cooled to -30°C, washed with cold isopentane, dried in vac. at 0°C; elem. anal.;

Reference yield:

: 10170-61-3
tetraethyl ammonium pentacarbonyl (triphenyl phosphine) vanadat

: 72622-82-3
V(CO)5{P(C₆H₅)3}

Guidance literature:: With tropylium tetrafluoroborate; In toluene; byproducts: [Et4N][BF4], (C7H7)2; stirring for 12 h at 243°K; filtration, washing with toluene, evapn. of combined toluene soln., evapn. to dryness (273°K, 1 Torr), washing with pentane (200. degree.K), drying under high vac. (6 h, 273°K);
DOI:10.1016/S0022-328X(00)81017-7