tetraethyl ammonium pentacarbonyl (triphenyl phosphine) vanadat

Base Information

Chemical Name:tetraethyl ammonium pentacarbonyl (triphenyl phosphine) vanadat
CAS No.:10170-61-3
Molecular Formula:C₈H₂₀N*C₂₃H₁₅O₅PV
Molecular Weight:583.538
Hs Code.:

Synonyms:tetraethyl ammonium pentacarbonyl (triphenyl phosphine) vanadat

Suppliers and Price of tetraethyl ammonium pentacarbonyl (triphenyl phosphine) vanadat

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetraethyl ammonium pentacarbonyl (triphenyl phosphine) vanadat

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of tetraethyl ammonium pentacarbonyl (triphenyl phosphine) vanadat

There total 6 articles about tetraethyl ammonium pentacarbonyl (triphenyl phosphine) vanadat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 3Na⁽¹⁺⁾*V(CO)5^(3-)=Na₃V(CO)5

: 71-91-0
tetraethylammonium bromide

: 10170-61-3
tetraethyl ammonium pentacarbonyl (triphenyl phosphine) vanadat

Guidance literature:: With ammonia; triphenylphosphine; In tetrahydrofuran; ammonia; PPh3 and (C2H5)4NBr added to complex soln. in liq. NH3 at -78°C,THF (-60°C) added, warmed slowly to room temp.; solvent removed (vac.), triturated with isopentane, dried, THF added, filtered, evapd., recrystd. (acetone/Et2O), washed with EtOH and Et2O, dried (vac.);

Reference yield: 73.0%

: 72622-82-3
V(CO)5{P(C₆H₅)3}

: 71-91-0
tetraethylammonium bromide

: 10170-61-3
tetraethyl ammonium pentacarbonyl (triphenyl phosphine) vanadat

Guidance literature:: With Na/Hg; In acetone; toluene; under N2 stirring for 12 h, toluene removed in vac., solid dissolved inacetone, reacted with Et4NBr;

Reference yield: 30.0%

: 20644-87-5
(hexacarbonyl)vanadinate^(1-)

: 66-40-0
tetraethyl ammonium

: 603-35-0
triphenylphosphine

: 10170-61-3
tetraethyl ammonium pentacarbonyl (triphenyl phosphine) vanadat

Guidance literature:: With hydrogenchloride; sodium amalgam; In benzene; V(CO)6(1-) salts is mixed vith P(C6H5)3 in molar ratio 1:2; 4 N HCl is added, from the red benzene phase Na salt is pptd. with Na amalgam; Na salt is converted with (C2H5)4N(1+) salt;