N,N'-bis<3-<(benzyloxycarbonyl)amino>propyl>-3-pentanediamide

Base Information

Chemical Name:N,N'-bis<3-<(benzyloxycarbonyl)amino>propyl>-3-pentanediamide
CAS No.:85185-25-7
Molecular Formula:C₃₅H₄₃N₅O₈
Molecular Weight:661.755
Hs Code.:

N,N'-bis<3-<(benzyloxycarbonyl)amino>propyl>-3-<N-(benzyloxycarbonyl)amino>pentanediamide

Synonyms:N,N'-bis<3-<(benzyloxycarbonyl)amino>propyl>-3-pentanediamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-bis<3-<(benzyloxycarbonyl)amino>propyl>-3-pentanediamide

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Technology Process of N,N'-bis<3-<(benzyloxycarbonyl)amino>propyl>-3-pentanediamide

There total 3 articles about N,N'-bis<3-<(benzyloxycarbonyl)amino>propyl>-3-pentanediamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 46460-73-5
N-benzyloxycarbonyl-1,3-diaminopropane

: 17336-01-5
3-pentanedioic acid

: 85185-25-7
N,N'-bis<3-<(benzyloxycarbonyl)amino>propyl>-3-pentanediamide

Guidance literature:: With diethyl cyanophosphonate; triethylamine; In N,N-dimethyl-formamide; 1.) 20 deg C, 1 h, 2.) 100 deg C, 30 min;
DOI:10.1021/jm00151a011

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 85185-25-7
N,N'-bis<3-<(benzyloxycarbonyl)amino>propyl>-3-pentanediamide

Guidance literature:: Multi-step reaction with 2 steps

1: 39 percent / KHCOO₃ / H₂O; bis-(2-methoxy-ethyl) ether / 4 h / 20 °C

2: 72 percent / diethyl phosphorocyanidate, Et₃N / dimethylformamide / 1.) 20 deg C, 1 h, 2.) 100 deg C, 30 min

With diethyl cyanophosphonate; potassium hydrogencarbonate; triethylamine; In diethylene glycol dimethyl ether; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00151a011

Reference yield:

: 3-aminoglutaric acid hydrochloride

: 85185-25-7
N,N'-bis<3-<(benzyloxycarbonyl)amino>propyl>-3-pentanediamide

Guidance literature:: Multi-step reaction with 2 steps

1: 39 percent / KHCOO₃ / H₂O; bis-(2-methoxy-ethyl) ether / 4 h / 20 °C

2: 72 percent / diethyl phosphorocyanidate, Et₃N / dimethylformamide / 1.) 20 deg C, 1 h, 2.) 100 deg C, 30 min

With diethyl cyanophosphonate; potassium hydrogencarbonate; triethylamine; In diethylene glycol dimethyl ether; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00151a011