N-CARBOBENZOXY-1,3-DIAMINOPROPANE HYDROCHLORIDE

Base Information

• Chemical Name: N-CARBOBENZOXY-1,3-DIAMINOPROPANE HYDROCHLORIDE
• CAS No.: 46460-73-5
• Molecular Formula: C11H16N2O2
• Molecular Weight: 208.26
• Hs Code.: 2924299090
• Mol file: 46460-73-5.mol

Synonyms:N-Carbobenzoxy-1,3-diaminopropane hydrochloride;TIMTEC-BB SBB003190;N-Z-1,3-Diaminopropane hydrochloride;N-Cbz-1,3-diaminopropane hydrochloride;N1-Benzyloxycarbonyl-1,3-diaminopropane hydrochloride;N-1-Carbobenzoxy-1,3-diaminopropane hydrochloride;N-1-Z-1,3-Diaminopropane HCl;N-(3-Aminopropyl)carbamic acid benzyl ester hydrochloride;N-Carbobenzoxy-1,3-diaminopropane hydrochloride;Z-NH(CH2)3NH2 HCl;Z-1,3-Diaminopropane HCl;Z-Diaminopropane HCl;Z-DAP HCL;Benzyl N-(3-aminopropyl)carbamate hydrochloride;

Chemical Property of N-CARBOBENZOXY-1,3-DIAMINOPROPANE HYDROCHLORIDE

Chemical Property:

• Melting Point: 185-189 °C
• Boiling Point: 368.2 °C at 760 mmHg
• PKA: 12.52±0.46(Predicted)
• Flash Point: 176.5 °C
• PSA: 67.84000
• Density: 1.109 g/cm³
• LogP: 2.16630
• Storage Temp.: Keep in dark place,Inert atmosphere,Store in freezer, under -20°C

Purity/Quality:

99%, ^*data from raw suppliers

Benzyl(3-aminopropyl)carbamate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

• Uses: N-Carbobenzoxy-1,3-diaminopropane, HCl

Technology Process of N-CARBOBENZOXY-1,3-DIAMINOPROPANE HYDROCHLORIDE

There total 13 articles about N-CARBOBENZOXY-1,3-DIAMINOPROPANE HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

N-(tert-butoxycarbonyl)-N'-(benzyloxycarbonyl)-1,3-propanediamine (160291-51-0) → N-benzyloxycarbonyl-1,3-diaminopropane (46460-73-5)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 4h;

DOI:10.1016/S0968-0896(01)00356-X

Reference yield: 93.0%

C22H34N4O6 (168827-62-1) → N-benzyloxycarbonyl-1,3-diaminopropane (46460-73-5)

Guidance literature:

With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol; for 3h;

DOI:10.1021/jm981013e

Reference yield: 80.0%

N-(Benzyloxycarbonyloxy)succinimide (13139-17-8) + Trimethylenediamine (109-76-2,54018-94-9) → N-benzyloxycarbonyl-1,3-diaminopropane (46460-73-5)

Guidance literature:

In chloroform; Ambient temperature;

DOI:10.1021/jm00045a003

upstream raw materials:

N,N'-Dicarbobenzoxy-1,3-diaminopropan

benzyl chloroformate

Trimethylenediamine

N-(Benzyloxycarbonyloxy)succinimide

Downstream raw materials:

N,N'-bis<3-<(benzyloxycarbonyl)amino>propyl>pentanediamide

(3-{[5-(3-Benzyloxycarbonylamino-propylcarbamoyl)-2-methyl-2H-pyrazole-3-carbonyl]-amino}-propyl)-carbamic acid benzyl ester

[3-(3-Benzyloxycarbonylamino-propylcarbamoyl)-propyl]-carbamic acid tert-butyl ester

[3-(3-Benzyloxycarbonylamino-propionylamino)-propyl]-carbamic acid benzyl ester

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