3-(1-(4-tert-butylphenethyl)-2-oxo-1,2,5,6-tetrahydropyridin-3-yl)-N-hydroxypropanamide

Base Information

Chemical Name:3-(1-(4-tert-butylphenethyl)-2-oxo-1,2,5,6-tetrahydropyridin-3-yl)-N-hydroxypropanamide
CAS No.:1258215-59-6
Molecular Formula:C₂₀H₂₈N₂O₃
Molecular Weight:344.454
Hs Code.:

Synonyms:3-(1-(4-tert-butylphenethyl)-2-oxo-1,2,5,6-tetrahydropyridin-3-yl)-N-hydroxypropanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(1-(4-tert-butylphenethyl)-2-oxo-1,2,5,6-tetrahydropyridin-3-yl)-N-hydroxypropanamide

Chemical Property:

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Technology Process of 3-(1-(4-tert-butylphenethyl)-2-oxo-1,2,5,6-tetrahydropyridin-3-yl)-N-hydroxypropanamide

There total 6 articles about 3-(1-(4-tert-butylphenethyl)-2-oxo-1,2,5,6-tetrahydropyridin-3-yl)-N-hydroxypropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 1291075-53-0
methyl 3-(1-(4-tert-butylphenethyl)-2-oxo-1,2,5,6-tetrahydropyridin-3-yl)propanoate

: 1258215-59-6
3-(1-(4-tert-butylphenethyl)-2-oxo-1,2,5,6-tetrahydropyridin-3-yl)-N-hydroxypropanamide

Guidance literature:: With hydroxylamine potassium salt; In methanol; at 0 ℃;
DOI:10.1002/cmdc.201300393

Reference yield:

: 93633-32-0
5-methoxy-2-methylene-5-oxopentanoic acid

: 1258215-59-6
3-(1-(4-tert-butylphenethyl)-2-oxo-1,2,5,6-tetrahydropyridin-3-yl)-N-hydroxypropanamide

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane

2: Grubbs catalyst first generation / dichloromethane

3: hydroxylamine potassium salt / methanol / 0 °C

With Grubbs catalyst first generation; dmap; hydroxylamine potassium salt; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane;
DOI:10.1016/j.bmcl.2010.08.117

Reference yield:

: 1258215-83-6
N-(4-tert-butylphenethyl)but-3-en-1-amine

: 1258215-59-6
3-(1-(4-tert-butylphenethyl)-2-oxo-1,2,5,6-tetrahydropyridin-3-yl)-N-hydroxypropanamide

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane

2: Grubbs catalyst first generation / dichloromethane

3: hydroxylamine potassium salt / methanol / 0 °C

With Grubbs catalyst first generation; dmap; hydroxylamine potassium salt; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane;
DOI:10.1016/j.bmcl.2010.08.117