Phenyl 1-(4-methylphenyl)propyl ketone

Base Information

Chemical Name:Phenyl 1-(4-methylphenyl)propyl ketone
CAS No.:146790-89-8
Molecular Formula:C₁₇H₁₈O
Molecular Weight:238.329
Hs Code.:

Synonyms:Phenyl 1-(4-methylphenyl)propyl ketone

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Chemical Property of Phenyl 1-(4-methylphenyl)propyl ketone

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Technology Process of Phenyl 1-(4-methylphenyl)propyl ketone

There total 10 articles about Phenyl 1-(4-methylphenyl)propyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 99-99-0
1-methyl-4-nitrobenzene

: 495-40-9
propiophenone

: 146790-89-8
Phenyl 1-(4-methylphenyl)propyl ketone

Guidance literature:: With potassium phosphate; bis(acetylacetonato)palladium(II); dicyclohexyl-(2′,4′,6′-triisopropyl-3,6-dimethoxy-[1,1′-biphenyl]-2-yl)phosphine; In cyclohexane; at 130 ℃; for 24h; Inert atmosphere;
DOI:10.1021/acs.orglett.0c04104

Reference yield: 53.0%

: 4-trimethylammonium-toluene trifluoromethanesulfonate

: 495-40-9
propiophenone

: 146790-89-8
Phenyl 1-(4-methylphenyl)propyl ketone

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; 1,3-bis(2,6-diisopropylphenyl)imidazolium chloride; lithium tert-butoxide; In tetrahydrofuran; at 80 ℃; for 24h; Schlenk technique; Inert atmosphere;
DOI:10.1039/c6ob01299j

Reference yield:

: 77134-00-0
(E)-4-methylcinnamyl acetate

: 146790-89-8
Phenyl 1-(4-methylphenyl)propyl ketone

Guidance literature:: Multi-step reaction with 2 steps

1: bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; tricyclohexylphosphine / ethyl acetate / 12 h / 60 °C / Inert atmosphere; Sealed tube

2: chloro(1,5-cyclooctadiene)rhodium(I) dimer; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; potassium hydrogen difluoride / hexane; methanol / 15 h / 70 °C / Inert atmosphere; Glovebox; Sealed tube

With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; chloro(1,5-cyclooctadiene)rhodium(I) dimer; potassium hydrogen difluoride; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tricyclohexylphosphine; In methanol; hexane; ethyl acetate;
DOI:10.1002/chem.202103851