N-[4-(6-chloro-3-pyridinyl)phenyl]-N'-[4-(4-quinazolinyloxy)phenyl]sulfamide

Base Information

Chemical Name:N-[4-(6-chloro-3-pyridinyl)phenyl]-N'-[4-(4-quinazolinyloxy)phenyl]sulfamide
CAS No.:1018833-04-9
Molecular Formula:C₂₅H₁₈ClN₅O₃S
Molecular Weight:503.969
Hs Code.:

Synonyms:N-[4-(6-chloro-3-pyridinyl)phenyl]-N'-[4-(4-quinazolinyloxy)phenyl]sulfamide

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Chemical Property of N-[4-(6-chloro-3-pyridinyl)phenyl]-N'-[4-(4-quinazolinyloxy)phenyl]sulfamide

Chemical Property:

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Technology Process of N-[4-(6-chloro-3-pyridinyl)phenyl]-N'-[4-(4-quinazolinyloxy)phenyl]sulfamide

There total 3 articles about N-[4-(6-chloro-3-pyridinyl)phenyl]-N'-[4-(4-quinazolinyloxy)phenyl]sulfamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1018833-42-5
N-[4-(6-chloro-3-pyridinyl)phenyl]-2-oxo-1,3-oxazolidine-3-sulfonamide

: 1018833-43-6
4-(quinazolin-4-yloxy)aniline hydrochloride

: 1018833-04-9
N-[4-(6-chloro-3-pyridinyl)phenyl]-N'-[4-(4-quinazolinyloxy)phenyl]sulfamide

Guidance literature:: With triethylamine; In acetonitrile; at 80 ℃; for 11h; Heating / reflux;

Reference yield:

: 106-40-1
4-bromo-aniline

: 1018833-04-9
N-[4-(6-chloro-3-pyridinyl)phenyl]-N'-[4-(4-quinazolinyloxy)phenyl]sulfamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium phosphate; tricyclohexylphosphine / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane; water / 18 h / 100 °C

2.1: dichloromethane / 1 h / 0 °C

2.2: 1.75 h / 0 - 20 °C

3.1: triethylamine / acetonitrile / 11 h / 80 °C / Heating / reflux

With potassium phosphate; triethylamine; tricyclohexylphosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In 1,4-dioxane; dichloromethane; water; acetonitrile; 1.1: Suzuki Coupling;

Reference yield:

: 444120-91-6
6-chloropyridin-3-ylboronic acid

: 1018833-04-9
N-[4-(6-chloro-3-pyridinyl)phenyl]-N'-[4-(4-quinazolinyloxy)phenyl]sulfamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium phosphate; tricyclohexylphosphine / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane; water / 18 h / 100 °C

2.1: dichloromethane / 1 h / 0 °C

2.2: 1.75 h / 0 - 20 °C

3.1: triethylamine / acetonitrile / 11 h / 80 °C / Heating / reflux

With potassium phosphate; triethylamine; tricyclohexylphosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In 1,4-dioxane; dichloromethane; water; acetonitrile; 1.1: Suzuki Coupling;