N-Benzyloxycarbonyl-N^ε-tert-butyloxycarbonyl-L-lysylglycyl-L-asparaginyl-L-leucyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamyl-L-arginyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamic Acid α-Methyl Ester p-Toluenesulfonate Salt

Base Information

• Chemical Name: N-Benzyloxycarbonyl-N^ε-tert-butyloxycarbonyl-L-lysylglycyl-L-asparaginyl-L-leucyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamyl-L-arginyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamic Acid α-Methyl Ester p-Toluenesulfonate Salt
• CAS No.: 87136-49-0
• Molecular Formula: C₇H₈O₃S*C₆₆H₁₀₈N₁₂O₂₁
• Molecular Weight: 1577.86

Synonyms:N-Benzyloxycarbonyl-N^ε-tert-butyloxycarbonyl-L-lysylglycyl-L-asparaginyl-L-leucyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamyl-L-arginyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamic Acid α-Methyl Ester p-Toluenesulfonate Salt

Chemical Property of N-Benzyloxycarbonyl-N^ε-tert-butyloxycarbonyl-L-lysylglycyl-L-asparaginyl-L-leucyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamyl-L-arginyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamic Acid α-Methyl Ester p-Toluenesulfonate Salt

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of N-Benzyloxycarbonyl-N^ε-tert-butyloxycarbonyl-L-lysylglycyl-L-asparaginyl-L-leucyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamyl-L-arginyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamic Acid α-Methyl Ester p-Toluenesulfonate Salt

There total 1 articles about N-Benzyloxycarbonyl-N^ε-tert-butyloxycarbonyl-L-lysylglycyl-L-asparaginyl-L-leucyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamyl-L-arginyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamic Acid α-Methyl Ester p-Toluenesulfonate Salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

Nα-Benzyloxycarbonyl-Nε-tert-butyloxycarbonyl-L-lysylglycyl-L-asparaginyl-L-leucine Lithium Salt (87136-46-7) + γ,γ-Di-tert-butyl-L-γ-carboxyglutamyl-L-arginyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamic Acid α-Methyl Ester p-Toluenesulfonate Salt (87136-47-8) → N-Benzyloxycarbonyl-Nε-tert-butyloxycarbonyl-L-lysylglycyl-L-asparaginyl-L-leucyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamyl-L-arginyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamic Acid α-Methyl Ester p-Toluenesulfonate Salt (87136-49-0)

Guidance literature:

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;

DOI:10.1021/jo00170a015

Reference yield: 98.0%

N-Benzyloxycarbonyl-Nε-tert-butyloxycarbonyl-L-lysylglycyl-L-asparaginyl-L-leucyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamyl-L-arginyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamic Acid α-Methyl Ester p-Toluenesulfonate Salt (87136-49-0) + trifluoroacetic acid (76-05-1) → Nα-Benzyloxycarbonyl-L-lysylglycyl-L-asparaginyl-L-leucyl-L-γ-carboxyglutamyl-L-arginyl-L-γ-carboxyglutamic Acid α-Methyl Ester p-Toluenesulfonate Trifluoracetate Mixed Salt (87136-53-6)

Guidance literature:

In acetic acid; for 36h; Ambient temperature;

DOI:10.1021/jo00170a015

upstream raw materials:

N^α-Benzyloxycarbonyl-N^ε-tert-butyloxycarbonyl-L-lysylglycyl-L-asparaginyl-L-leucine Lithium Salt

γ,γ-Di-tert-butyl-L-γ-carboxyglutamyl-L-arginyl-γ,γ-di-tert-butyl-L-γ-carboxyglutamic Acid α-Methyl Ester p-Toluenesulfonate Salt

Downstream raw materials:

N^α-Benzyloxycarbonyl-L-lysylglycyl-L-asparaginyl-L-leucyl-L-γ-carboxyglutamyl-L-arginyl-L-γ-carboxyglutamic Acid α-Methyl Ester p-Toluenesulfonate Trifluoracetate Mixed Salt

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