1-<4-(methoxycarbonyl)benzyl>-8,15,22-trimethyl-1,8,15,22-tetraazoniatricyclo<13,13,6,6^8,22>tetracontane tetrakis(tetrafluoroborate)

Base Information

• Chemical Name: 1-<4-(methoxycarbonyl)benzyl>-8,15,22-trimethyl-1,8,15,22-tetraazoniatricyclo<13,13,6,6^8,22>tetracontane tetrakis(tetrafluoroborate)
• CAS No.: 105206-50-6
• Molecular Formula: 4BF₄*C₄₈H₉₀N₄O₂
• Molecular Weight: 1102.49

Synonyms:1-<4-(methoxycarbonyl)benzyl>-8,15,22-trimethyl-1,8,15,22-tetraazoniatricyclo<13,13,6,6^8,22>tetracontane tetrakis(tetrafluoroborate)

Chemical Property of 1-<4-(methoxycarbonyl)benzyl>-8,15,22-trimethyl-1,8,15,22-tetraazoniatricyclo<13,13,6,6^8,22>tetracontane tetrakis(tetrafluoroborate)

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Technology Process of 1-<4-(methoxycarbonyl)benzyl>-8,15,22-trimethyl-1,8,15,22-tetraazoniatricyclo<13,13,6,6^8,22>tetracontane tetrakis(tetrafluoroborate)

There total 3 articles about 1-<4-(methoxycarbonyl)benzyl>-8,15,22-trimethyl-1,8,15,22-tetraazoniatricyclo<13,13,6,6^8,22>tetracontane tetrakis(tetrafluoroborate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

1-<<4-(methoxycarbonyl)benzyl>azonia>-8,15,22-triazatricyclo<13.13.6.68,22>tetracontane iodide (94224-93-8) + methyl iodide (74-88-4) → 1-<4-(methoxycarbonyl)benzyl>-8,15,22-trimethyl-1,8,15,22-tetraazoniatricyclo<13,13,6,68,22>tetracontane tetrakis(tetrafluoroborate) (105206-50-6)

Guidance literature:

With sodium carbonate; In acetonitrile; at 70 ℃; for 3h;

DOI:10.1021/jo00376a021

Reference yield:

1,8,15,22-Tetraazatricyclo<13.13.6.68,22>tetracontan (63702-67-0) → 1-<4-(methoxycarbonyl)benzyl>-8,15,22-trimethyl-1,8,15,22-tetraazoniatricyclo<13,13,6,68,22>tetracontane tetrakis(tetrafluoroborate) (105206-50-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / diethyl ether / 336 h / 4 °C

2: 74 percent / Na₂CO₃ / acetonitrile / 3 h / 70 °C

With sodium carbonate; In diethyl ether; acetonitrile;

DOI:10.1021/jo00376a021

Reference yield:

methyl 4-(iodomethyl)benzoate (94224-92-7) → 1-<4-(methoxycarbonyl)benzyl>-8,15,22-trimethyl-1,8,15,22-tetraazoniatricyclo<13,13,6,68,22>tetracontane tetrakis(tetrafluoroborate) (105206-50-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / diethyl ether / 336 h / 4 °C

2: 74 percent / Na₂CO₃ / acetonitrile / 3 h / 70 °C

With sodium carbonate; In diethyl ether; acetonitrile;

DOI:10.1021/jo00376a021

upstream raw materials:

1-<<4-(methoxycarbonyl)benzyl>azonia>-8,15,22-triazatricyclo<13.13.6.6^8,22>tetracontane iodide

methyl iodide

1,8,15,22-Tetraazatricyclo<13.13.6.6^8,22>tetracontan

methyl 4-(iodomethyl)benzoate

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