2-(3,4-dimethoxyphenyl)-4-(3-isopropoxy-4-methoxyphenyl)-4-oxobutyric acid

Base Information

Chemical Name:2-(3,4-dimethoxyphenyl)-4-(3-isopropoxy-4-methoxyphenyl)-4-oxobutyric acid
CAS No.:88114-47-0
Molecular Formula:C₂₂H₂₆O₇
Molecular Weight:402.444
Hs Code.:

Synonyms:2-(3,4-dimethoxyphenyl)-4-(3-isopropoxy-4-methoxyphenyl)-4-oxobutyric acid

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Chemical Property of 2-(3,4-dimethoxyphenyl)-4-(3-isopropoxy-4-methoxyphenyl)-4-oxobutyric acid

Chemical Property:

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Technology Process of 2-(3,4-dimethoxyphenyl)-4-(3-isopropoxy-4-methoxyphenyl)-4-oxobutyric acid

There total 6 articles about 2-(3,4-dimethoxyphenyl)-4-(3-isopropoxy-4-methoxyphenyl)-4-oxobutyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.9%

: 88114-46-9
2-(3,4-dimethoxyphenyl)-4-(3-isopropoxy-4-methoxyphenyl)-4-oxobutyronitrile

: 88114-47-0
2-(3,4-dimethoxyphenyl)-4-(3-isopropoxy-4-methoxyphenyl)-4-oxobutyric acid

Guidance literature:: With sodium hydroxide; water; In ethanol; for 7.5h; Heating;
DOI:10.1248/cpb.31.2963

Reference yield:

: 621-59-0
isovanillin

: 88114-47-0
2-(3,4-dimethoxyphenyl)-4-(3-isopropoxy-4-methoxyphenyl)-4-oxobutyric acid

Guidance literature:: Multi-step reaction with 6 steps

1: 88 percent / potassium carbonate / dimethylformamide

3: Jones reagent

4: sodium hydroxide / aq. ethanol

5: 75.5 percent / acetic acid / 2-ethoxy-ethanol

6: 95.9 percent / sodium hydroxide, H₂O / ethanol / 7.5 h / Heating

With sodium hydroxide; jones reagent; water; potassium carbonate; acetic acid; In 2-ethoxy-ethanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.31.2963

Reference yield:

: 34123-66-5
O-isopropylisovanillin

: 88114-47-0
2-(3,4-dimethoxyphenyl)-4-(3-isopropoxy-4-methoxyphenyl)-4-oxobutyric acid

Guidance literature:: Multi-step reaction with 5 steps

2: Jones reagent

3: sodium hydroxide / aq. ethanol

4: 75.5 percent / acetic acid / 2-ethoxy-ethanol

5: 95.9 percent / sodium hydroxide, H₂O / ethanol / 7.5 h / Heating

With sodium hydroxide; jones reagent; water; acetic acid; In 2-ethoxy-ethanol; ethanol;
DOI:10.1248/cpb.31.2963