2-(3,4-dimethoxyphenyl)-6-hydroxy-7-methoxy-1-(N-methylformamido)naphthalene

Base Information

Chemical Name:2-(3,4-dimethoxyphenyl)-6-hydroxy-7-methoxy-1-(N-methylformamido)naphthalene
CAS No.:88114-55-0
Molecular Formula:C₂₁H₂₁NO₅
Molecular Weight:367.401
Hs Code.:

Synonyms:2-(3,4-dimethoxyphenyl)-6-hydroxy-7-methoxy-1-(N-methylformamido)naphthalene

Suppliers and Price of 2-(3,4-dimethoxyphenyl)-6-hydroxy-7-methoxy-1-(N-methylformamido)naphthalene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2-(3,4-dimethoxyphenyl)-6-hydroxy-7-methoxy-1-(N-methylformamido)naphthalene

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Hazard Codes:

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Technology Process of 2-(3,4-dimethoxyphenyl)-6-hydroxy-7-methoxy-1-(N-methylformamido)naphthalene

There total 20 articles about 2-(3,4-dimethoxyphenyl)-6-hydroxy-7-methoxy-1-(N-methylformamido)naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.7%

: 88114-54-9
2-(3,4-dimethoxyphenyl)-6-isopropoxy-7-methoxy-1-(N-methylformamido)naphthalene

: 88114-55-0
2-(3,4-dimethoxyphenyl)-6-hydroxy-7-methoxy-1-(N-methylformamido)naphthalene

Guidance literature:: With sulfuric acid; In acetic acid;
DOI:10.1248/cpb.31.2963

Reference yield:

: 88114-45-8
3'-isopropoxy-3,4,4'-trimethoxychalcone

: 88114-55-0
2-(3,4-dimethoxyphenyl)-6-hydroxy-7-methoxy-1-(N-methylformamido)naphthalene

Guidance literature:: Multi-step reaction with 9 steps

1: 75.5 percent / acetic acid / 2-ethoxy-ethanol

2: 95.9 percent / sodium hydroxide, H₂O / ethanol / 7.5 h / Heating

3: H₂ / 10percent palladium-charcoal

4: 71 percent / phosphorus oxychloride / CHCl₃ / 2.5 h / 80 °C

5: titanium tetrachloride / CHCl₃ / -5 - 0 °C

6: sodium borohydride

7: 88.1 percent

8: 87.1 percent / 2,3-dichloro-5,6-dicyano-p-benzoquinone / benzene

9: 80.7 percent / conc. sulfuric acid / acetic acid

With sodium hydroxide; sodium tetrahydroborate; sulfuric acid; water; hydrogen; titanium tetrachloride; acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; trichlorophosphate; palladium on activated charcoal; In 2-ethoxy-ethanol; ethanol; chloroform; acetic acid; benzene;
DOI:10.1248/cpb.31.2963

Reference yield:

: 88114-47-0
2-(3,4-dimethoxyphenyl)-4-(3-isopropoxy-4-methoxyphenyl)-4-oxobutyric acid

: 88114-55-0
2-(3,4-dimethoxyphenyl)-6-hydroxy-7-methoxy-1-(N-methylformamido)naphthalene

Guidance literature:: Multi-step reaction with 7 steps

1: H₂ / 10percent palladium-charcoal

2: 71 percent / phosphorus oxychloride / CHCl₃ / 2.5 h / 80 °C

3: titanium tetrachloride / CHCl₃ / -5 - 0 °C

4: sodium borohydride

5: 88.1 percent

6: 87.1 percent / 2,3-dichloro-5,6-dicyano-p-benzoquinone / benzene

7: 80.7 percent / conc. sulfuric acid / acetic acid

With sodium tetrahydroborate; sulfuric acid; hydrogen; titanium tetrachloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; trichlorophosphate; palladium on activated charcoal; In chloroform; acetic acid; benzene;
DOI:10.1248/cpb.31.2963