methanesulfonic acid 2-[5-(tert-butoxycarbonylaminophenyl-methyl)-tetrazol-1-yl]-1-(tert-butyl-diphenylsilanyloxymethyl)-ethyl ester

Base Information

Chemical Name:methanesulfonic acid 2-[5-(tert-butoxycarbonylaminophenyl-methyl)-tetrazol-1-yl]-1-(tert-butyl-diphenylsilanyloxymethyl)-ethyl ester
CAS No.:1187063-72-4
Molecular Formula:C₃₃H₄₃N₅O₆SSi
Molecular Weight:665.886
Hs Code.:

Synonyms:methanesulfonic acid 2-[5-(tert-butoxycarbonylaminophenyl-methyl)-tetrazol-1-yl]-1-(tert-butyl-diphenylsilanyloxymethyl)-ethyl ester

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Chemical Property of methanesulfonic acid 2-[5-(tert-butoxycarbonylaminophenyl-methyl)-tetrazol-1-yl]-1-(tert-butyl-diphenylsilanyloxymethyl)-ethyl ester

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Technology Process of methanesulfonic acid 2-[5-(tert-butoxycarbonylaminophenyl-methyl)-tetrazol-1-yl]-1-(tert-butyl-diphenylsilanyloxymethyl)-ethyl ester

There total 1 articles about methanesulfonic acid 2-[5-(tert-butoxycarbonylaminophenyl-methyl)-tetrazol-1-yl]-1-(tert-butyl-diphenylsilanyloxymethyl)-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1187063-71-3
({1-[3-(tert-butyl-diphenyl-silanyloxy)-2-hydroxy-propyl]-1H-tetrazol-5-yl}-phenyl-methyl)-carbamic acid tert-butyl ester

: 7143-01-3
Methanesulfonic anhydride

: 1187063-72-4
methanesulfonic acid 2-[5-(tert-butoxycarbonylaminophenyl-methyl)-tetrazol-1-yl]-1-(tert-butyl-diphenylsilanyloxymethyl)-ethyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 24h;
DOI:10.1016/j.tet.2009.06.033

Reference yield:

: 1187063-72-4
methanesulfonic acid 2-[5-(tert-butoxycarbonylaminophenyl-methyl)-tetrazol-1-yl]-1-(tert-butyl-diphenylsilanyloxymethyl)-ethyl ester

: C₂₈H₃₅N₅O₄SSi

Guidance literature:: methanesulfonic acid 2-[5-(tert-butoxycarbonylaminophenyl-methyl)-tetrazol-1-yl]-1-(tert-butyl-diphenylsilanyloxymethyl)-ethyl ester; With trifluoroacetic acid; In dichloromethane; at -15 - 20 ℃; for 3h;

With sodium hydrogencarbonate; In dichloromethane; Saturated solution;
DOI:10.1016/j.tet.2009.06.033