4-chloroacetophenone enol trifluoroacetate

Base Information

• Chemical Name: 4-chloroacetophenone enol trifluoroacetate
• CAS No.: 54265-96-2
• Molecular Formula: C₁₀H₆ClF₃O₂
• Molecular Weight: 250.605

Synonyms:4-chloroacetophenone enol trifluoroacetate

Chemical Property of 4-chloroacetophenone enol trifluoroacetate

Chemical Property:

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Technology Process of 4-chloroacetophenone enol trifluoroacetate

There total 1 articles about 4-chloroacetophenone enol trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trifluoroacetyl bromide (354-31-4) + C8H6Cl2HgO → 4-chloroacetophenone enol trifluoroacetate (54265-96-2)

Guidance literature:

In 1,2-dichloro-ethane;

DOI:10.1016/S0022-328X(00)86453-0

Reference yield: 60.0%

4-chloroacetophenone enol trifluoroacetate (54265-96-2) + (t-C4H9)2SbOCH3 (53742-69-1) → (t-C4H9)2SbCH2COC6H4-4-Cl (54266-08-9) + trifluoroacetic acid-methyl ester (431-47-0)

Guidance literature:

at 0°C, in argon; isolation by vac. distn.;

DOI:10.1016/S0022-328X(00)86453-0

Reference yield: 60.0%

4-chloroacetophenone enol trifluoroacetate (54265-96-2) + (t-C4H9)2SbOCH3 (53742-69-1) → (t-C4H9)2SbCH2COC6H4-4-Cl (54266-08-9)

Guidance literature:

0°C, 2h;

DOI:10.1016/S0022-328X(00)86453-0

upstream raw materials:

trifluoroacetyl bromide

Downstream raw materials:

(t-C₄H₉)2SbCH₂COC₆H₄-4-Cl

trifluoroacetic acid-methyl ester

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