C₉H₁₂N₄

Base Information

Chemical Name:C₉H₁₂N₄
CAS No.:1380230-82-9
Molecular Formula:C₉H₁₂N₄
Molecular Weight:176.221
Hs Code.:

C<sub>9</sub>H<sub>12</sub>N<sub>4</sub>

Synonyms:C₉H₁₂N₄

Suppliers and Price of C₉H₁₂N₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₉H₁₂N₄

Chemical Property:

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Technology Process of C₉H₁₂N₄

There total 6 articles about C₉H₁₂N₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1380230-80-7
C₁₇H₁₄N₄O₂

: 1380230-82-9
C₉H₁₂N₄

Guidance literature:: With hydrazine hydrate; In methanol; for 4h; Reflux;
DOI:10.1021/ol3012106

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 1380230-82-9
C₉H₁₂N₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / -20 °C / Inert atmosphere

1.2: 0.33 h / -20 °C / Inert atmosphere

2.1: trifluoroacetic acid / 0.5 h

3.1: imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; potassium carbonate / methanol / 20 °C

4.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere

5.1: hydrazine hydrate / methanol / 4 h / Reflux

With 4-methyl-morpholine; imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; di-isopropyl azodicarboxylate; potassium carbonate; hydrazine hydrate; triphenylphosphine; isobutyl chloroformate; In tetrahydrofuran; methanol; trifluoroacetic acid; 4.1: Mitsunobu reaction;
DOI:10.1021/ol3012106

Reference yield:

: 66605-57-0
(S)-N-tert-butoxycarbonyl-2-amino-3-phenylpropanol

: 1380230-82-9
C₉H₁₂N₄

Guidance literature:: Multi-step reaction with 4 steps

1: trifluoroacetic acid / 0.5 h

2: imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; potassium carbonate / methanol / 20 °C

3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere

4: hydrazine hydrate / methanol / 4 h / Reflux

With imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; di-isopropyl azodicarboxylate; potassium carbonate; hydrazine hydrate; triphenylphosphine; In tetrahydrofuran; methanol; trifluoroacetic acid; 3: Mitsunobu reaction;
DOI:10.1021/ol3012106