(2S,3R,4R,5S)-2-(N-p-toluenesulfonyl)aminomethyl-3,4-dibenzyloxy-5-benzyloxymethylpyrrolidine

Base Information

• Chemical Name: (2S,3R,4R,5S)-2-(N-p-toluenesulfonyl)aminomethyl-3,4-dibenzyloxy-5-benzyloxymethylpyrrolidine
• CAS No.: 1226778-58-0
• Molecular Formula: C₃₄H₃₈N₂O₅S
• Molecular Weight: 586.752

Synonyms:(2S,3R,4R,5S)-2-(N-p-toluenesulfonyl)aminomethyl-3,4-dibenzyloxy-5-benzyloxymethylpyrrolidine

Chemical Property of (2S,3R,4R,5S)-2-(N-p-toluenesulfonyl)aminomethyl-3,4-dibenzyloxy-5-benzyloxymethylpyrrolidine

Chemical Property:

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Technology Process of (2S,3R,4R,5S)-2-(N-p-toluenesulfonyl)aminomethyl-3,4-dibenzyloxy-5-benzyloxymethylpyrrolidine

There total 2 articles about (2S,3R,4R,5S)-2-(N-p-toluenesulfonyl)aminomethyl-3,4-dibenzyloxy-5-benzyloxymethylpyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

(2S,3R,4R,5S)-2-(N-p-toluenesulfonyl)aminomethyl-3,4-dibenzyloxy-5-benzyloxymethyl-1N-(p-tolenesulfonyl)pyrrolidine (1226778-55-7) → (2S,3R,4R,5S)-2-(N-p-toluenesulfonyl)aminomethyl-3,4-dibenzyloxy-5-benzyloxymethylpyrrolidine (1226778-58-0)

Guidance literature:

With disodium hydrogenphosphate; sodium; mercury; In methanol; N,N-dimethyl-formamide; at 60 ℃; for 3h; chemoselective reaction; Inert atmosphere;

DOI:10.1039/b926123k

Reference yield: 83.0%

(2S,3R,4R,5S)-2-(N-acetyl-N-p-toluenesulfonyl)aminomethyl-3,4-dibenzyloxy-5-benzyloxymethyl-1N-(p-tolenesulfonyl)pyrrolidine (1226778-57-9) → (2S,3R,4R,5S)-2-(N-p-toluenesulfonyl)aminomethyl-3,4-dibenzyloxy-5-benzyloxymethylpyrrolidine (1226778-58-0)

Guidance literature:

With disodium hydrogenphosphate; sodium; mercury; In methanol; N,N-dimethyl-formamide; at 60 ℃; for 3h; chemoselective reaction; Inert atmosphere;

DOI:10.1039/b926123k

Reference yield: 90.0%

(2S,3R,4R,5S)-2-(N-p-toluenesulfonyl)aminomethyl-3,4-dibenzyloxy-5-benzyloxymethylpyrrolidine (1226778-58-0) → (2S,3R,4R,5S)-2-(N-p-toluenesulfonyl)aminomethyl-3,4-dihydroxy-5-hydroxymethylpyrrolidine (1226778-59-1)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In methanol; at 30 ℃; for 5h;

DOI:10.1039/b926123k

upstream raw materials:

(2S,3R,4R,5S)-2-(N-acetyl-N-p-toluenesulfonyl)aminomethyl-3,4-dibenzyloxy-5-benzyloxymethyl-1N-(p-tolenesulfonyl)pyrrolidine

(2S,3R,4R,5S)-2-(N-p-toluenesulfonyl)aminomethyl-3,4-dibenzyloxy-5-benzyloxymethyl-1N-(p-tolenesulfonyl)pyrrolidine

Downstream raw materials:

(2S,3R,4R,5S)-2-(N-p-toluenesulfonyl)aminomethyl-3,4-dihydroxy-5-hydroxymethylpyrrolidine

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