5-((3R,4R)-5-((tert-butyldiphenylsilyl)oxy)-4-methylpent-1-en-3-yl)-2-methoxy-3-methylphenol

Base Information

Chemical Name:5-((3R,4R)-5-((tert-butyldiphenylsilyl)oxy)-4-methylpent-1-en-3-yl)-2-methoxy-3-methylphenol
CAS No.:1414861-43-0
Molecular Formula:C₃₀H₃₈O₃Si
Molecular Weight:474.715
Hs Code.:

Synonyms:5-((3R,4R)-5-((tert-butyldiphenylsilyl)oxy)-4-methylpent-1-en-3-yl)-2-methoxy-3-methylphenol

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Chemical Property of 5-((3R,4R)-5-((tert-butyldiphenylsilyl)oxy)-4-methylpent-1-en-3-yl)-2-methoxy-3-methylphenol

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Technology Process of 5-((3R,4R)-5-((tert-butyldiphenylsilyl)oxy)-4-methylpent-1-en-3-yl)-2-methoxy-3-methylphenol

There total 1 articles about 5-((3R,4R)-5-((tert-butyldiphenylsilyl)oxy)-4-methylpent-1-en-3-yl)-2-methoxy-3-methylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1414861-42-9
tert-Butyl[((2R,3R)-3-(4-methoxy-3-methyl-5-((R,E)-pent-3-en-2-yloxy)phenyl)-2-methylpent-4-en-1-yl)oxy]diphenylsilane tert-Butyl[((2R,3R)-3-(4-methoxy-3-methyl-5-((R,E)-pent-3-en-2-yloxy)phenyl)-2-methylpent-4-en-1-yl)oxy]diphenylsilane tert-Butyl[((2R,3R)-3-(4-methoxy-3-methyl-5-((R,E)-pent-3-en-2-yloxy)phenyl)-2-methylpent-4-en-1-yl)oxy]diphenylsilane tert-butyl[((2R,3R)-3-(4-methoxy-3-methyl-5-((R,E)-pent-3-en-2-yloxy)phenyl)-2-methylpent-4-en-1-yl)oxy]diphenylsilane

: 1414861-44-1
3-((3R,4R)-5-((tert-butyldiphenylsilyl)oxy)-4-methylpent-1-en-3-yl)-6-methoxy-5-methyl-2-((S,E)-pent-3-en-2-yl)phenol

: 1414861-45-2
3-((3R,4R)-5-((tert-Butyldiphenylsilyl)oxy)-4-methylpent-1-en-3-yl)-6-methoxy-5-methyl-2-((R,E)-pent-3-en-2-yl)phenol

: 1414861-43-0
5-((3R,4R)-5-((tert-butyldiphenylsilyl)oxy)-4-methylpent-1-en-3-yl)-2-methoxy-3-methylphenol

Guidance literature:: With tris(6,6,7,7,8,8-heptafluoro-2,2-dimethyl-3,5-octadionato)europium(III); In toluene; at 120 ℃; for 22h; Inert atmosphere;
DOI:10.1055/s-0032-1316643

Reference yield: 95.0%

: pent-3-en-2-yl (2,2,2-trichloroethyl) carbonate

: 1414861-43-0
5-((3R,4R)-5-((tert-butyldiphenylsilyl)oxy)-4-methylpent-1-en-3-yl)-2-methoxy-3-methylphenol

: 1414861-42-9
tert-Butyl[((2R,3R)-3-(4-methoxy-3-methyl-5-((R,E)-pent-3-en-2-yloxy)phenyl)-2-methylpent-4-en-1-yl)oxy]diphenylsilane tert-Butyl[((2R,3R)-3-(4-methoxy-3-methyl-5-((R,E)-pent-3-en-2-yloxy)phenyl)-2-methylpent-4-en-1-yl)oxy]diphenylsilane tert-Butyl[((2R,3R)-3-(4-methoxy-3-methyl-5-((R,E)-pent-3-en-2-yloxy)phenyl)-2-methylpent-4-en-1-yl)oxy]diphenylsilane tert-butyl[((2R,3R)-3-(4-methoxy-3-methyl-5-((R,E)-pent-3-en-2-yloxy)phenyl)-2-methylpent-4-en-1-yl)oxy]diphenylsilane

Guidance literature:: With [Pd₂(dba)3]*CHCl₃; (R,R)-DACH-Ph; In dichloromethane; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1055/s-0032-1316643