N²-<4-(methylamino)benzoyl>-2-amino-3-<<(methylamino)carbonyl>amino>propanoic acid

Base Information

• Chemical Name: N²-<4-(methylamino)benzoyl>-2-amino-3-<<(methylamino)carbonyl>amino>propanoic acid
• CAS No.: 96846-08-1
• Molecular Formula: C₁₃H₁₈N₄O₄
• Molecular Weight: 294.31

Synonyms:N²-<4-(methylamino)benzoyl>-2-amino-3-<<(methylamino)carbonyl>amino>propanoic acid

Chemical Property of N²-<4-(methylamino)benzoyl>-2-amino-3-<<(methylamino)carbonyl>amino>propanoic acid

Chemical Property:

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Technology Process of N²-<4-(methylamino)benzoyl>-2-amino-3-<<(methylamino)carbonyl>amino>propanoic acid

There total 4 articles about N²-<4-(methylamino)benzoyl>-2-amino-3-<<(methylamino)carbonyl>amino>propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N2-<4-<<(benzyloxy)carbonyl>methylamino>benzoyl>-2-amino-3-<<(methylamino)carbonyl>amino>propanoic acid (96846-05-8) → N2-<4-(methylamino)benzoyl>-2-amino-3-<<(methylamino)carbonyl>amino>propanoic acid (96846-08-1)

Guidance literature:

With hydrogen; palladium on activated charcoal; In acetic acid; at 25 ℃; for 3.5h; under 2324.2 Torr; Yield given;

DOI:10.1021/jm00146a008

Reference yield:

benzyl (4-(chlorocarbonyl)phenyl)(methyl)carbamate (66891-86-9) → N2-<4-(methylamino)benzoyl>-2-amino-3-<<(methylamino)carbonyl>amino>propanoic acid (96846-08-1)

Guidance literature:

Multi-step reaction with 2 steps

1: (i-Pr)2NEt / dioxane; H₂O

2: H₂ / 30percent Pd/C / acetic acid / 3.5 h / 25 °C / 2324.2 Torr

With hydrogen; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In 1,4-dioxane; water; acetic acid;

DOI:10.1021/jm00146a008

Reference yield:

N2-<(4-methylphenyl)sulfonyl>-2-amino-3-<<(methylamino)carbonyl>amino>propanoic acid (96846-01-4) → N2-<4-(methylamino)benzoyl>-2-amino-3-<<(methylamino)carbonyl>amino>propanoic acid (96846-08-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 30percent HBr, CH₃COOH, phenol / 96 h

2: (i-Pr)2NEt / dioxane; H₂O

3: H₂ / 30percent Pd/C / acetic acid / 3.5 h / 25 °C / 2324.2 Torr

With hydrogen bromide; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; phenol; palladium on activated charcoal; In 1,4-dioxane; water; acetic acid;

DOI:10.1021/jm00146a008

upstream raw materials:

N²-<4-<<(benzyloxy)carbonyl>methylamino>benzoyl>-2-amino-3-<<(methylamino)carbonyl>amino>propanoic acid

benzyl (4-(chlorocarbonyl)phenyl)(methyl)carbamate

N²-<(4-methylphenyl)sulfonyl>-2-amino-3-<<(methylamino)carbonyl>amino>propanoic acid

2-amino-3-<<(methylamino)carbonyl>amino>propanoic acid hydrobromide

Downstream raw materials:

N-²-<4-<<(2,4-diamino-6-pteridinyl)methyl>methylamino>benzoyl>-3-<<(methylamino)carbonyl>amino>propanoic acid

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