C₃₆H₂₈O₅

Base Information

Chemical Name:C₃₆H₂₈O₅
CAS No.:1388829-28-4
Molecular Formula:C₃₆H₂₈O₅
Molecular Weight:540.615
Hs Code.:

C<sub>36</sub>H<sub>28</sub>O<sub>5</sub>

Synonyms:C₃₆H₂₈O₅

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Chemical Property of C₃₆H₂₈O₅

Chemical Property:

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Technology Process of C₃₆H₂₈O₅

There total 8 articles about C₃₆H₂₈O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1141892-88-7
(((4-ethynyl-1,2-phenylene)bis(oxy))bis(methylene))dibenzene

: 1388829-24-0
4-(benzyloxy)-3-hydroxy-2-iodobenzaldehyde

: 1388829-28-4
C₃₆H₂₈O₅

Guidance literature:: (((4-ethynyl-1,2-phenylene)bis(oxy))bis(methylene))dibenzene; 4-(benzyloxy)-3-hydroxy-2-iodobenzaldehyde; With bis-triphenylphosphine-palladium(II) chloride; triethylamine; In N,N-dimethyl-formamide; for 0.25h;

With copper(l) iodide; at 65 ℃; for 12h; Inert atmosphere;
DOI:10.3998/ark.5550190.0013.619

Reference yield:

: 100-39-0
benzyl bromide

: 1388829-28-4
C₃₆H₂₈O₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

2.1: iodine; silver sulfate / ethanol; dichloromethane / 1 h / 20 °C

3.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 12 h / 20 °C / Inert atmosphere

4.1: methanol; potassium carbonate / 24 h / 20 °C

5.1: bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 0.25 h

5.2: 12 h / 65 °C / Inert atmosphere

With methanol; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; iodine; potassium carbonate; silver sulfate; triethylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide; 3.1: Sonogashira coupling / 5.1: Sonogashira coupling / 5.2: Sonogashira coupling;
DOI:10.3998/ark.5550190.0013.619

Reference yield:

: 100-44-7
benzyl chloride

: 1388829-28-4
C₃₆H₂₈O₅

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogencarbonate; sodium iodide / N,N-dimethyl-formamide / 48 h / 40 °C

2.1: pyridine; Iodine monochloride / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

3.1: bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 0.25 h

3.2: 12 h / 65 °C / Inert atmosphere

With pyridine; bis-triphenylphosphine-palladium(II) chloride; Iodine monochloride; sodium hydrogencarbonate; triethylamine; sodium iodide; In dichloromethane; N,N-dimethyl-formamide; 3.1: Sonogashira coupling / 3.2: Sonogashira coupling;
DOI:10.3998/ark.5550190.0013.619