lithium 1-methyl-o-carborane

Base Information

Chemical Name:lithium 1-methyl-o-carborane
CAS No.:32630-05-0
Molecular Formula:C₃H₁₃B₁₀Li
Molecular Weight:164.187
Hs Code.:

Synonyms:lithium 1-methyl-o-carborane

Suppliers and Price of lithium 1-methyl-o-carborane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of lithium 1-methyl-o-carborane

Chemical Property:

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Technology Process of lithium 1-methyl-o-carborane

There total 1 articles about lithium 1-methyl-o-carborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-72-8,29786-93-4
n-butyllithium

: 23940-18-3
1-(Hg-o-CB₁₀H₁₀CCH₃)-2-(CH₃)-1.2-C₂B₁₀H₁₀

: 32630-05-0
1-lithio-2-methyl-o-carborane

: 629-35-6
dibutylmercury

Guidance literature:

Reference yield: 91.0%

: 32630-05-0
lithium 1-methyl-o-carborane

: 138500-85-3
4-bromomethylphenylboronic acid pinacol ester

: 920317-27-7
B₁₀H₁₀C₂CH₃CH₂C₆H₄BO₂C₂(CH₃)4

Guidance literature:: In not given; bromomethylboronic ester reacted with lithium anion of 1-methyl-o-carborane;
DOI:10.1039/b611571c

Reference yield: 80.0%

: 32630-05-0
1-lithio-2-methyl-o-carborane

: 16070-58-9
tris(triphenylphosphine)chloroiridium

: [IrCl(H)(C₆H₄PPh₂)(triphenylphosphane)₂]

Guidance literature:: In not given; Ar-atmosphere; addn. of equimolar amt. of borane to suspn. of Ir-complexin THF, C6H6 or Et2O (not specified), stirring (0°C, 1 h, pptn.); filtration, recrystn. CH2Cl2/Et2O);
DOI:10.1016/S0020-1693(00)95676-7