endo-9-benzyl-7,8-diaza-1,9-dimethyl-6-phenyltricyclo<4.2.1.0^2,5>non-7-ene

Base Information

Chemical Name:endo-9-benzyl-7,8-diaza-1,9-dimethyl-6-phenyltricyclo<4.2.1.0^2,5>non-7-ene
CAS No.:74971-31-6
Molecular Formula:C₂₂H₂₄N₂
Molecular Weight:316.446
Hs Code.:

endo-9-benzyl-7,8-diaza-1,9-dimethyl-6-phenyltricyclo<4.2.1.0<sup>2,5</sup>>non-7-ene

Synonyms:endo-9-benzyl-7,8-diaza-1,9-dimethyl-6-phenyltricyclo<4.2.1.0^2,5>non-7-ene

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Chemical Property of endo-9-benzyl-7,8-diaza-1,9-dimethyl-6-phenyltricyclo<4.2.1.0^2,5>non-7-ene

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Technology Process of endo-9-benzyl-7,8-diaza-1,9-dimethyl-6-phenyltricyclo<4.2.1.0^2,5>non-7-ene

There total 6 articles about endo-9-benzyl-7,8-diaza-1,9-dimethyl-6-phenyltricyclo<4.2.1.0^2,5>non-7-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 74971-26-9
endo-9-benzyl-7,8-diaza-1,9-dimethyl-6-phenyltricyclo<4.2.1.0^2,5>nona-3,7-diene

: 74971-31-6
endo-9-benzyl-7,8-diaza-1,9-dimethyl-6-phenyltricyclo<4.2.1.0^2,5>non-7-ene

Guidance literature:: With potassium diazodicarboxylate; acetic acid; In methanol; for 0.5h;
DOI:10.1021/ja00533a018

Reference yield:

: 28918-08-3
2-benzyl-1-phenylbutane-1,3-dione

: 74971-31-6
endo-9-benzyl-7,8-diaza-1,9-dimethyl-6-phenyltricyclo<4.2.1.0^2,5>non-7-ene

Guidance literature:: Multi-step reaction with 4 steps

1: 58.8 percent / sodium hydride / dimethylsulfoxide

2: 69 percent / hydrazine hydrate / CCl₄ / 1 h / Heating

3: 30.2 percent / ceric ammonium nitrate / acetone / 0.5 h / -20 °C

4: 90 percent / dipotassium azodicarboxylate, acetic acid / methanol / 0.5 h

With ammonium cerium(IV) nitrate; potassium diazodicarboxylate; sodium hydride; hydrazine hydrate; acetic acid; In methanol; tetrachloromethane; dimethyl sulfoxide; acetone;
DOI:10.1021/ja00533a018

Reference yield:

: 60433-18-3
2-benzyl-2-methyl-1-phenyl-butane-1,3-dione

: 74971-31-6
endo-9-benzyl-7,8-diaza-1,9-dimethyl-6-phenyltricyclo<4.2.1.0^2,5>non-7-ene

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / hydrazine hydrate / CCl₄ / 1 h / Heating

2: 30.2 percent / ceric ammonium nitrate / acetone / 0.5 h / -20 °C

3: 90 percent / dipotassium azodicarboxylate, acetic acid / methanol / 0.5 h

With ammonium cerium(IV) nitrate; potassium diazodicarboxylate; hydrazine hydrate; acetic acid; In methanol; tetrachloromethane; acetone;
DOI:10.1021/ja00533a018