3-Amino-5-hydroxybenzoic acid, N-CBZ protected

Base Information

• Chemical Name: 3-Amino-5-hydroxybenzoic acid, N-CBZ protected
• CAS No.: 900799-69-1
• Molecular Formula: C15H13 N O5
• Molecular Weight: 287.272
• Hs Code.: 2924299090
• Mol file: 900799-69-1.mol

Synonyms:3-(Benzyloxycarbonylamino)-5-hydroxy-benzoicacid

Chemical Property of 3-Amino-5-hydroxybenzoic acid, N-CBZ protected

Chemical Property:

• Vapor Pressure: 2.9E-10mmHg at 25°C
• Melting Point: 216-220.5oC
• Boiling Point: 486.2oC at 760 mmHg
• Flash Point: 247.8oC
• PSA: 95.86000
• Density: 1.432g/cm3
• LogP: 2.91210

Purity/Quality:

97% ^*data from raw suppliers

3-([(BENZYLOXY)CARBONYL]AMINO)-5-HYDROXYBENZOIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Amino-5-hydroxybenzoic acid, N-CBZ protected

There total 1 articles about 3-Amino-5-hydroxybenzoic acid, N-CBZ protected which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

3-amino-5-hydroxybenzoic acid (76045-71-1) + benzyl chloroformate (501-53-1,94274-21-2) → 3-Benzyloxycarbonylamino-5-hydroxy-benzoic acid (900799-69-1)

Guidance literature:

3-amino-5-hydroxybenzoic acid; benzyl chloroformate; With sodium carbonate; In tetrahydrofuran; water; at 20 ℃; for 20h;

With hydrogenchloride; In tetrahydrofuran; diethyl ether; water;

upstream raw materials:

3-amino-5-hydroxybenzoic acid

benzyl chloroformate