rac-2-(3-(3-isothiocyanatopyridin-4-yl)cyclohex-2-en-1-yl)isoindoline-1,3-dione

Base Information

Chemical Name:rac-2-(3-(3-isothiocyanatopyridin-4-yl)cyclohex-2-en-1-yl)isoindoline-1,3-dione
CAS No.:1405128-61-1
Molecular Formula:C₂₀H₁₅N₃O₂S
Molecular Weight:361.424
Hs Code.:

Synonyms:rac-2-(3-(3-isothiocyanatopyridin-4-yl)cyclohex-2-en-1-yl)isoindoline-1,3-dione

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Chemical Property of rac-2-(3-(3-isothiocyanatopyridin-4-yl)cyclohex-2-en-1-yl)isoindoline-1,3-dione

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Technology Process of rac-2-(3-(3-isothiocyanatopyridin-4-yl)cyclohex-2-en-1-yl)isoindoline-1,3-dione

There total 2 articles about rac-2-(3-(3-isothiocyanatopyridin-4-yl)cyclohex-2-en-1-yl)isoindoline-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 1405128-60-0
rac-(3-(3-azidopyridin-4-yl)cyclohex-2-en-1-yl)isoindoline-1,3-dione

: 1405128-61-1
rac-2-(3-(3-isothiocyanatopyridin-4-yl)cyclohex-2-en-1-yl)isoindoline-1,3-dione

Guidance literature:: rac-(3-(3-azidopyridin-4-yl)cyclohex-2-en-1-yl)isoindoline-1,3-dione; With trimethylphosphane; In tetrahydrofuran; at -5 ℃; for 0.5h; Inert atmosphere;

carbon disulfide; In tetrahydrofuran; at -5 ℃; Inert atmosphere;

Reference yield:

: 1187055-84-0
2-[3-(3-nitropyridin-4-yl)cyclohex-2-en-1-yl]-1H-isoindole-1,3(2H)-dione

: 1405128-61-1
rac-2-(3-(3-isothiocyanatopyridin-4-yl)cyclohex-2-en-1-yl)isoindoline-1,3-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen / palladium 10% on activated carbon / 2,2,2-trifluoroethanol / 12 h / 206.87 Torr / Inert atmosphere

2.1: sodium azide; sodium nitrite; sulfuric acid / water; acetone / -5 °C

2.2: 0.5 h

3.1: trimethylphosphane / tetrahydrofuran / 0.5 h / -5 °C / Inert atmosphere

3.2: -5 °C / Inert atmosphere

With sodium azide; sulfuric acid; hydrogen; sodium nitrite; trimethylphosphane; palladium 10% on activated carbon; In tetrahydrofuran; 2,2,2-trifluoroethanol; water; acetone;

Reference yield:

: 1405127-64-1
3-(azidomethyl)-6-(2,6-difluorophenyl)pyridazine

: 1405128-61-1
rac-2-(3-(3-isothiocyanatopyridin-4-yl)cyclohex-2-en-1-yl)isoindoline-1,3-dione

: 1405129-08-9
rac-2-(3-(3-((2-(2,6-difluorophenyl)imidazo[1,5-b]pyridazin-7-yl)amino)pyridin-4-yl)cyclohex-2-en-1-yl)isoindoline-1,3-dione

Guidance literature:: 3-(azidomethyl)-6-(2,6-difluorophenyl)pyridazine; With trimethylphosphane; In tetrahydrofuran; at -5 ℃; for 0.75h; Inert atmosphere;

rac-2-(3-(3-isothiocyanatopyridin-4-yl)cyclohex-2-en-1-yl)isoindoline-1,3-dione; In tetrahydrofuran;