N-glycine methyl ester disulfide

Base Information

Chemical Name:N-glycine methyl ester disulfide
CAS No.:24948-53-6
Molecular Formula:C₂₈H₃₄N₄O₁₀S₂
Molecular Weight:650.731
Hs Code.:

N-<N-(benzyloxycarbonyl)cysteinyl>glycine methyl ester disulfide

Synonyms:N-glycine methyl ester disulfide

Suppliers and Price of N-glycine methyl ester disulfide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-glycine methyl ester disulfide

Chemical Property:

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Technology Process of N-glycine methyl ester disulfide

There total 10 articles about N-glycine methyl ester disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.4%

: {2-amino-3-[2-amino-2-(methoxycarbonylmethylcarbamoyl)ethyldisulfanyl]propionylamino}acetic acid methyl ester dihydrochloride

: 501-53-1,94274-21-2
benzyl chloroformate

: 24948-53-6
N-glycine methyl ester disulfide

Guidance literature:: With dmap; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/chem.201501458

Reference yield:

: 56-89-3
L-cystine

: 24948-53-6
N-glycine methyl ester disulfide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / dicyclohexylcarbodiimide; Et₃N / CH₂Cl₂ / 0 - 20 °C

With triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; 1: condensation / 2: condensation;
DOI:10.1016/S0968-0896(00)00257-1

Reference yield:

: 6968-11-2
N,N'-bis(benzyloxycarbonyl)-L-cystine

: 24948-53-6
N-glycine methyl ester disulfide

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 0.33 h

2: 1.) Et₃N, 2.) Et₃N, MeOH / 1.) CH₂Cl₂, 45 min, 2.) 2 d

With methanol; triethylamine; In dichloromethane;
DOI:10.1021/jo00273a031